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Quality Control Report <br />McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts" <br />Client:AdvancedGeo, Inc. <br />Project:Pilkington <br />Date Analyzed:02/04/2021 - 02/05/2021 <br />Date Prepared:02/03/2021 <br />WorkOrder:2102062 <br />BatchID:214440 <br />Analytical Method:SW8270C <br />Unit:mg/Kg <br />Sample ID:MB/LCS/LCSD-214440 <br />2102062-008AMS/MSD <br />Instrument:GC17, GC21 <br />Matrix:Soil <br />Extraction Method:SW3550B <br />QC Summary Report for SW8270C <br />Analyte LCS <br />Result <br />LCSD <br />Result <br />SPK <br />Val <br />LCS <br />%REC <br />LCSD <br />%REC <br />LCS/LCSD <br />Limits <br />RPD RPD <br />Limit <br />1,1-Biphenyl 0.0567 0.0509 0.062 91 81 60-130 10.9 30 <br />1,2,4-Trichlorobenzene 1.16 1.04 1.25 93 83 60-130 11.0 30 <br />1,2-Dichlorobenzene 1.24 1.15 1.25 99 92 60-130 7.19 30 <br />1,2-Diphenylhydrazine 1.25 1.08 1.25 100 86 60-130 14.9 30 <br />1,3-Dichlorobenzene 1.16 1.08 1.25 93 87 60-130 6.59 30 <br />1,4-Dichlorobenzene 1.11 1.04 1.25 89 83 60-130 6.55 30 <br />1-Methylnaphthalene 0.0735 0.0695 0.062 118 111 70-130 5.57 30 <br />2,3,4,6-Tetrachlorophenol 1.06 0.916 1.25 85 73 60-130 14.8 30 <br />2,4,5-Trichlorophenol 0.0595 0.0568 0.062 95 91 60-130 4.58 30 <br />2,4,6-Trichlorophenol 0.0569 0.0556 0.062 91 89 60-130 2.20 30 <br />2,4-Dichlorophenol 0.0686 0.0623 0.062 110 100 60-130 9.63 30 <br />2,4-Dimethylphenol 1.28 1.16 1.25 103 93 70-130 10.4 30 <br />2,4-Dinitrophenol 0.707 0.610 1.25 57 49 15-130 14.8 30 <br />2,4-Dinitrotoluene 0.0582 0.0501 0.062 93 80 70-130 14.9 30 <br />2,6-Dinitrotoluene 0.0532 0.0504 0.062 85 81 60-130 5.57 30 <br />2-Chloronaphthalene 1.23 1.04 1.25 98 83 60-130 16.6 30 <br />2-Chlorophenol 0.0619 0.0570 0.062 99 91 60-130 8.19 30 <br />2-Methylnaphthalene 0.0564 0.0576 0.062 90 92 70-130 2.08 30 <br />2-Methylphenol (o-Cresol)1.34 1.16 1.25 107 93 60-130 14.2 30 <br />2-Nitroaniline 6.79 5.97 6.25 109 96 70-130 12.9 30 <br />2-Nitrophenol 6.29 5.50 6.25 101 88 70-130 13.3 30 <br />3 & 4-Methylphenol (m,p-Cresol)1.36 1.24 1.25 109 99 60-130 9.57 30 <br />3,3-Dichlorobenzidine 0.0422 0.0404 0.062 68 65 40-130 4.32 30 <br />3-Nitroaniline 5.88 5.01 6.25 94 80 50-130 16.0 30 <br />4,6-Dinitro-2-methylphenol 4.59 4.05 6.25 73 65 20-130 12.6 30 <br />4-Bromophenyl Phenyl Ether 1.09 0.930 1.25 87 74 60-130 16.1 30 <br />4-Chloro-3-methylphenol 1.15 1.02 1.25 92 82 70-130 11.2 30 <br />4-Chloroaniline 0.0516 0.0445 0.062 83 71 40-130 14.7 30 <br />4-Chlorophenyl Phenyl Ether 1.12 0.951 1.25 89 76 70-130 15.8 30 <br />4-Nitroaniline 6.63 5.74 6.25 106 92 60-130 14.4 30 <br />4-Nitrophenol 5.17 4.74 6.25 83 76 60-130 8.55 30 <br />Acenaphthene 0.0744 0.0656 0.062 119 105 60-130 12.5 30 <br />Acenaphthylene 0.0496 0.0420 0.062 79 67 60-130 16.6 30 <br />Acetochlor 1.42 1.14 1.25 113 91 60-130 21.9 30 <br />Anthracene 0.0791 0.0670 0.062 127 107 60-130 16.6 30 <br />Benzidine 2.78 2.27 6.25 44 36 20-130 19.9 30 <br />Benzo (a) anthracene 0.0697 0.0600 0.062 112 96 70-130 15.0 30 <br />Benzo (a) pyrene 0.0616 0.0539 0.062 98 86 70-130 13.3 30 <br />CA ELAP 1644 • NELAP 4033ORELAP <br />(Cont.) <br />Page 127 of 154