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Quality Control Report <br />McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts" <br />Client:AdvancedGeo, Inc. <br />Project:Pilkington <br />Date Analyzed:02/04/2021 - 02/05/2021 <br />Date Prepared:02/03/2021 <br />WorkOrder:2102062 <br />BatchID:214440 <br />Analytical Method:SW8270C <br />Unit:mg/Kg <br />Sample ID:MB/LCS/LCSD-214440 <br />2102062-008AMS/MSD <br />Instrument:GC17, GC21 <br />Matrix:Soil <br />Extraction Method:SW3550B <br />QC Summary Report for SW8270C <br />Analyte LCS <br />Result <br />LCSD <br />Result <br />SPK <br />Val <br />LCS <br />%REC <br />LCSD <br />%REC <br />LCS/LCSD <br />Limits <br />RPD RPD <br />Limit <br />Benzo (b) fluoranthene 0.0454 0.0400 0.062 73 64 60-130 12.5 30 <br />Benzo (g,h,i) perylene 0.0578 0.0541 0.062 92 87 70-130 6.49 30 <br />Benzo (k) fluoranthene 0.0644 0.0561 0.062 103 90 70-130 13.7 30 <br />Benzyl Alcohol 4.81 4.20 6.25 77 67,F2 70-130 13.6 30 <br />Bis (2-chloroethoxy) Methane 1.32 1.19 1.25 105 96 70-130 9.78 30 <br />Bis (2-chloroethyl) Ether 0.0490 0.0479 0.062 78 77 60-130 2.38 30 <br />Bis (2-chloroisopropyl) Ether 0.0510 0.0567 0.062 82 91 60-130 10.5 30 <br />Bis (2-ethylhexyl) Adipate 1.20 1.04 1.25 96 84 60-130 13.8 30 <br />Bis (2-ethylhexyl) Phthalate 0.0554 0.0489 0.062 89 78 60-130 12.3 30 <br />Butylbenzyl Phthalate 0.0612 0.0537 0.062 98 86 60-130 13.2 30 <br />Chrysene 0.0720 0.0622 0.062 115 100 70-130 14.6 30 <br />Dibenzo (a,h) anthracene 0.0579 0.0549 0.062 93 88 70-130 5.21 30 <br />Dibenzofuran 1.27 1.11 1.25 101 89 60-130 13.6 30 <br />Diethyl Phthalate 0.0606 0.0521 0.062 97 83 70-130 15.1 30 <br />Dimethyl Phthalate 0.0597 0.0512 0.062 96 82 70-130 15.5 30 <br />Di-n-butyl Phthalate 0.0547 0.0480 0.062 88 77 60-130 13.1 30 <br />Di-n-octyl Phthalate 0.0511 0.0466 0.062 82 74 60-130 9.40 30 <br />Fluoranthene 0.0599 0.0516 0.062 96 83 70-130 14.8 30 <br />Fluorene 0.0745 0.0651 0.062 119 104 60-130 13.5 30 <br />Hexachlorobenzene 0.0512 0.0483 0.062 82 77 70-130 5.87 30 <br />Hexachlorobutadiene 0.0622 0.0588 0.062 99 94 70-130 5.59 30 <br />Hexachlorocyclopentadiene 5.12 4.40 6.25 82 70 60-130 15.1 30 <br />Hexachloroethane 0.0564 0.0532 0.062 90 85 70-130 5.94 30 <br />Indeno (1,2,3-cd) pyrene 0.0526 0.0475 0.062 84 76 70-130 10.3 30 <br />Isophorone 1.12 1.02 1.25 89 81 60-130 9.44 30 <br />Naphthalene 0.0530 0.0481 0.062 85 77 70-130 9.67 30 <br />Nitrobenzene 1.35 1.18 1.25 108 95 60-130 13.0 30 <br />N-Nitrosodimethylamine 5.16 4.82 6.25 83 77 70-130 7.01 30 <br />N-Nitrosodi-n-propylamine 1.09 1.03 1.25 87 83 60-130 5.23 30 <br />N-Nitrosodiphenylamine 1.28 1.10 1.25 103 88 70-130 15.0 30 <br />Pentachlorophenol 0.246 0.227 0.31 79 73 50-130 8.10 30 <br />Phenanthrene 0.0609 0.0524 0.062 97 84 60-130 14.9 30 <br />Phenol 0.258 0.241 0.25 103 96 60-130 6.74 30 <br />Pyrene 0.0709 0.0606 0.062 113 97 70-130 15.7 30 <br />Pyridine 0.990 0.856 1.25 79 68 60-130 14.6 30 <br />CA ELAP 1644 • NELAP 4033ORELAP <br />(Cont.) <br />Page 128 of 154