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Quality Control Report <br />McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts" <br />Client:AdvancedGeo, Inc. <br />Project:Pilkington <br />Date Analyzed:02/04/2021 - 02/05/2021 <br />Date Prepared:02/03/2021 <br />WorkOrder:2102062 <br />BatchID:214440 <br />Analytical Method:SW8270C <br />Unit:mg/Kg <br />Sample ID:MB/LCS/LCSD-214440 <br />2102062-008AMS/MSD <br />Instrument:GC17, GC21 <br />Matrix:Soil <br />Extraction Method:SW3550B <br />QC Summary Report for SW8270C <br />Analyte MS <br />Result <br />MSD <br />Result <br />SPK <br />Val <br />SPKRef <br />Val <br />MS <br />%REC <br />MSD <br />%REC <br />MS/MSD <br /> Limits <br />RPD RPD <br />Limit <br />MS <br />DF <br />4-Chloro-3-methylphenol 1.15 1.06 1.25 ND<2.0 92 85 60-130 8.42 301 <br />4-Chloroaniline 0.0633 0.0641 0.062 ND<0.010 101 102 40-130 1.19 301 <br />4-Chlorophenyl Phenyl Ether 1.15 1.08 1.25 ND<2.0 92 86 60-130 5.95 301 <br />4-Nitroaniline 6.72 6.29 6.25 ND<10 107 101 60-130 6.54 301 <br />4-Nitrophenol 7.01 6.60 6.25 ND<10 112 106 60-130 6.00 301 <br />Acenaphthene 0.233 0.223 0.062 0.1549 125 109 60-130 4.40 301 <br />Acenaphthylene 0.0884 0.0835 0.062 0.01034 125 117 60-130 5.69 301 <br />Acetochlor 1.27 1.34 1.25 ND<2.0 101 107 60-130 5.60 301 <br />Anthracene 0.504 0.477 0.062 0.3857 190,F1 146,F1 60-130 5.51 301 <br />Benzidine 3.11 2.82 6.25 ND<10 50 45 20-130 9.78 301 <br />Benzo (a) anthracene 1.11 1.06 0.062 0.8706 384,F1 304,F1 60-130 4.62 301 <br />Benzo (a) pyrene 0.844 0.825 0.062 0.6694 280,F1 249,F1 60-130 2.35 301 <br />Benzo (b) fluoranthene 1.05 1.07 0.062 0.8596 303,F1 334,F1 60-130 1.84 301 <br />Benzo (g,h,i) perylene 0.596 0.571 0.062 0.4641 212,F1 171,F1 60-130 4.33 301 <br />Benzo (k) fluoranthene 0.509 0.566 0.062 0.4408 108 200,F1 60-130 10.6 301 <br />Benzyl Alcohol 4.22 4.27 6.25 ND<10 67 68 60-130 1.16 301 <br />Bis (2-chloroethoxy) Methane 1.18 1.12 1.25 ND<2.0 94 90 60-130 4.71 301 <br />Bis (2-chloroethyl) Ether 0.0858 0.0875 0.062 ND<0.010 137,F1 140,F1 60-130 1.87 301 <br />Bis (2-chloroisopropyl) Ether 0.141 0.130 0.062 ND<0.10 225,F1 208,F1 60-130 7.92 301 <br />Bis (2-ethylhexyl) Adipate 1.30 1.26 1.25 ND<2.0 104 100 60-130 3.78 301 <br />Bis (2-ethylhexyl) Phthalate 0.0909 0.0919 0.062 ND<0.20 145,F1 147,F1 60-130 1.06 301 <br />Butylbenzyl Phthalate 0.0736 0.0759 0.062 ND<0.20 118 121 60-130 3.16 301 <br />Chrysene 1.30 1.20 0.062 0.9809 518,F1 350,F1 60-130 8.39 301 <br />Dibenzo (a,h) anthracene 0.144 0.126 0.062 0.1015 67 39,F1 60-130 13.0 301 <br />Dibenzofuran 1.40 1.29 1.25 ND<2.0 112 103 60-130 8.44 301 <br />Diethyl Phthalate 0.0728 0.0638 0.062 ND<0.10 116 102 60-130 13.1 301 <br />Dimethyl Phthalate 0.0622 0.0596 0.062 ND<0.020 100 95 60-130 4.34 301 <br />Di-n-butyl Phthalate 0.0905 0.0916 0.062 ND<0.10 94 95 60-130 1.20 301 <br />Di-n-octyl Phthalate 0.0898 0.0883 0.062 ND<0.10 144,F1 141,F1 60-130 1.72 301 <br />Fluoranthene 3.28 3.12 0.062 2.665 977,F1 725,F1 60-130 4.92 301 <br />Fluorene 0.186 0.174 0.062 0.09623 143,F1 124 60-130 6.52 301 <br />Hexachlorobenzene 0.0704 0.0656 0.062 ND<0.020 113 105 60-130 6.94 301 <br />Hexachlorobutadiene 0.0735 0.0714 0.062 ND<0.010 118 114 60-130 3.02 301 <br />Hexachlorocyclopentadiene 3.42 3.22 6.25 ND<16 55,F1 52,F1 60-130 6.10 301 <br />Hexachloroethane 0.0801 0.0770 0.062 ND<0.10 128 123 60-130 3.98 301 <br />Indeno (1,2,3-cd) pyrene 0.547 0.546 0.062 0.4446 163,F1 163,F1 60-130 0.0649 301 <br />Isophorone 1.18 1.22 1.25 ND<2.0 94 97 60-130 3.22 301 <br />Naphthalene 0.0757 0.0727 0.062 ND<0.010 112 107 60-130 4.03 301 <br />CA ELAP 1644 • NELAP 4033ORELAP <br />(Cont.) <br />Page 130 of 154