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Quality Control Report <br />McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts" <br />Client:AdvancedGeo, Inc. <br />Project:Pilkington <br />Date Analyzed:02/04/2021 - 02/05/2021 <br />Date Prepared:02/03/2021 <br />WorkOrder:2102062 <br />BatchID:214440 <br />Analytical Method:SW8270C <br />Unit:mg/Kg <br />Sample ID:MB/LCS/LCSD-214440 <br />2102062-008AMS/MSD <br />Instrument:GC17, GC21 <br />Matrix:Soil <br />Extraction Method:SW3550B <br />QC Summary Report for SW8270C <br />Analyte LCS <br />Result <br />LCSD <br />Result <br />SPK <br />Val <br />LCS <br />%REC <br />LCSD <br />%REC <br />LCS/LCSD <br />Limits <br />RPD RPD <br />Limit <br />Surrogate Recovery <br />2-Fluorophenol 1.43 1.37 1.25 114 109 70-130 4.25 30 <br />Phenol-d5 1.31 1.27 1.25 105 101 70-130 3.74 30 <br />Nitrobenzene-d5 1.38 1.30 1.25 111 104 60-130 6.02 30 <br />2-Fluorobiphenyl 1.25 1.15 1.25 100 92 60-130 8.85 30 <br />2,4,6-Tribromophenol 1.13 1.01 1.25 90 81 30-130 10.9 30 <br />4-Terphenyl-d14 1.34 1.20 1.25 108 96 40-130 11.7 30 <br />Analyte MS <br />Result <br />MSD <br />Result <br />SPK <br />Val <br />SPKRef <br />Val <br />MS <br />%REC <br />MSD <br />%REC <br />MS/MSD <br /> Limits <br />RPD RPD <br />Limit <br />MS <br />DF <br />1,1-Biphenyl 0.0769 0.0738 0.062 ND<0.10 123 118 60-130 4.06 301 <br />1,2,4-Trichlorobenzene 1.15 1.14 1.25 ND<2.0 92 92 60-130 0.384 301 <br />1,2-Dichlorobenzene 1.31 1.29 1.25 ND<2.0 105 103 60-130 1.31 301 <br />1,2-Diphenylhydrazine 1.43 1.41 1.25 ND<2.0 114 113 60-130 1.07 301 <br />1,3-Dichlorobenzene 1.25 1.30 1.25 ND<2.0 100 104 60-130 4.24 301 <br />1,4-Dichlorobenzene 1.30 1.29 1.25 ND<2.0 104 103 60-130 0.894 301 <br />1-Methylnaphthalene 0.0645 0.0617 0.062 ND<0.010 90 86 60-130 4.36 301 <br />2,3,4,6-Tetrachlorophenol 0.552 0.651 1.25 ND<2.0 44,F1 52,F1 60-130 16.4 301 <br />2,4,5-Trichlorophenol 0.0628 0.0589 0.062 ND<0.020 101 94 60-130 6.45 301 <br />2,4,6-Trichlorophenol 0.0607 0.0597 0.062 ND<0.020 97 95 60-130 1.65 301 <br />2,4-Dichlorophenol 0.0522 0.0528 0.062 ND<0.010 84 84 60-130 1.06 301 <br />2,4-Dimethylphenol 1.22 1.15 1.25 ND<2.0 97 92 60-130 5.81 301 <br />2,4-Dinitrophenol 0.415 0.463 1.25 ND<2.0 33 37 15-130 10.9 301 <br />2,4-Dinitrotoluene 0.0686 0.0678 0.062 ND<0.10 110 108 60-130 1.19 301 <br />2,6-Dinitrotoluene 0.0836 0.0753 0.062 ND<0.10 134,F1 120 60-130 10.5 301 <br />2-Chloronaphthalene 1.32 1.14 1.25 ND<2.0 105 91 60-130 14.6 301 <br />2-Chlorophenol 0.0775 0.0765 0.062 ND<0.10 124 122 60-130 1.38 301 <br />2-Methylnaphthalene 0.0903 0.0867 0.062 0.01000 128 123 60-130 3.99 301 <br />2-Methylphenol (o-Cresol)1.42 1.51 1.25 ND<2.0 113 121 60-130 6.42 301 <br />2-Nitroaniline 9.01 8.88 6.25 ND<10 144,F1 142,F1 60-130 1.51 301 <br />2-Nitrophenol 8.56 8.33 6.25 ND<10 137,F1 133,F1 60-130 2.76 301 <br />3 & 4-Methylphenol (m,p-Cresol)1.43 1.28 1.25 ND<2.0 115 103 60-130 11.3 301 <br />3,3-Dichlorobenzidine 0.0740 0.0718 0.062 ND<0.020 118 115 40-130 3.01 301 <br />3-Nitroaniline 8.02 7.64 6.25 ND<10 128 122 50-130 4.87 301 <br />4,6-Dinitro-2-methylphenol 4.23 4.31 6.25 ND<10 68 69 20-130 1.98 301 <br />4-Bromophenyl Phenyl Ether 1.08 1.03 1.25 ND<2.0 86 82 60-130 5.17 301 <br />CA ELAP 1644 • NELAP 4033ORELAP <br />(Cont.) <br />Page 129 of 154