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TO E RO E K SOP No.026,REV.1 <br /> ASSOCIATES,INC INDOOR AIR AND SUB-SLAB SOIL GAS SAMPLING METHODS <br /> I PAGE 9 <br /> 7. Install and hydrate quick-drying Portland cement(no additives) in the annular space <br /> of the 3�4- to 1-inch hole. Allow the cement to dry according to manufacturer's <br /> instructions (typically 15 to 20 minutes). <br /> 8. Confirm the valve of the SUMMA®canister is closed and remove the brass cap.Attach <br /> the pressure gauge and flow controller (integrated system) to the canister.Attach the <br /> soil probe to the sample train with Teflon®or equivalent tubing. Note: some SUMMA® <br /> canister models utilize a quick-connect system and do not require the removal of <br /> brass caps. For quick-connect SUMMA® canisters, disregard further mentions of <br /> removal and replacement of the brass cap <br /> 9. Once fitted with the sampling tube, the ambient air within the sampling train is <br /> purged. Note: an optional and additional "T" valve assembly can be inserted into the <br /> sampling tube to serve as purge valve on/off switch if desired. Usually, 3 to 5 system <br /> volumes are purged prior to sample collection. If the sampling system purge volume <br /> cannot be measured, then a standard purge time of 3 to 5 minutes should be used. A <br /> PID may be used to purge ambient air while also providing a qualitative means to <br /> indicate when purging is complete (i.e., when VOCs are detected).A syringe may also <br /> be used to purge the sampling train a minimum of five times only if the volume of the <br /> syringe is greater that the sampling train and a secure shut off valve is installed a <br /> dosed properly between purge volumes. <br /> 10.After the system is purged of ambient air but before the pump is turned off, turn the <br /> purge "T"valve to the off position or if a"T"valve assembly is not being used, fold the <br /> sample tubing over itself(approximately 2 inches of the sampling line) closest to the <br /> entrance port of the pump. The tubing should be securely clamped to keep ambient <br /> air from reentering the system. After the purged system is sealed to ambient air, the <br /> pump should be turned off. Sample collection can now proceed using a SUMMA® <br /> canister. <br /> 11. Open the canister valve counterclockwise until fully opened, which will allow the <br /> evacuated canister to draw in soil gas, and immediately record the canister pressure <br /> reading and time.Also,record the initial vacuum of the canister. Note: some SUMMA® <br />