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The sampling procedure requires one end of the tubing to be been inserted into the ground a bentonite seal must be <br /> slipped over the sampling port and the other end over the formed between ambient air and the sample air. The <br /> canister nozzle or flow meter(if required) to acquire an air- bentonite must be hydrated and create an air tight seal <br /> tight connection. The valve should be opened at this time around the probe. If required IPA can be placed on the joints <br /> and the initial pressure should then be recorded to verify that of the vapor probe and analyzed for in the sample to ensure <br /> the Summa canister is under vacuum. The Summa canister that ambient air is not diluting the soil vapor survey samples. <br /> is allowed to collect the soil vapor sample at a <br /> predetermined duration. After the sample has been Once the sample apparatus has been set up new tubing will <br /> collected record the final vacuum reading (approximately five be connected to the inlet of the SKC sample pump. The <br /> pounds per square inch (psig))to ensure that the flow meter pump operates at a low flow purge rate of 200 milliliters per <br /> was working properly, if applicable. Immediately following minute to prevent air stripping of contaminants from the soil. <br /> the sample collection, complete sampling information is Once three volumes have been evacuated (minimum 4.2 <br /> recorded on the label on the air sampling canister(e.g., minutes of sample time) a sample can be collected. <br /> sample ID, date, time, location, and temperature). The Verification with a PID will determine when the maximum <br /> sample is placed in a non-refrigerated, dry cooler with concentration is obtained and a sample should be collected. <br /> sufficient packing to ensure against damage during If measurable concentrations are not obtained with the PID <br /> transport. Cooling samples will cause condensation of any after 7 purge volumes (10 minutes) a sample should be <br /> moisture within the air sample, thereby distorting laboratory collected. Once a sample has been determined to be <br /> analysis. collected new tubing will be placed on the effluent of the <br /> sample pump running to the Tedlar bag, which should be <br /> Summa canister samples are subject to hold times of filled to 3/4 of volume capacity. Caution should be taken not <br /> typically 30 days and with some compounds a more rigid to overfill the sampling bag. The sample is placed in a non- <br /> hold time of 14 days is required. refrigerated dry cooler with sufficient packing to eliminate <br /> damage during transport. Cooling samples will cause <br /> SOP-13 condensation of moisture within the sample, thereby <br /> SOIL VAPOR SAMPLING: SYRINGE SAMPLING distorting laboratory analysis. <br /> TECHNIQUE <br /> To minimize the potential for cross-contamination between <br /> Prior to vapor sampling, the vacuum system must reach a air samples new polyethylene tubing will be used for every <br /> stabilized air flow(cubic feet per minute) for approximately sample. <br /> 15 minutes. Prior to the actual collection of the vapor <br /> sample, the following data is recorded: air flow, temperature, Vapor samples are also subject to the same hold times and <br /> and pressure at collection ports and gauges. must be stored as stated in SOP-10. <br /> The sampling equipment consists of a clean, 100cc, gas- SOP-15 <br /> tight syringe and silicone septa. SOIL GAS SAMPLING FROM DIRECT PUSH SOIL <br /> BORING: "TEDLAR" BAG SAMPLING TECHNIQUE <br /> The sampling ports are brass connections, fitted with silicone <br /> septa, and threaded into a tapped hole in the system piping. To obtain soil gas samples from a direct push drill rig, <br /> Samples are collected by inserting a clean syringe into the advance a discreet sampling rod with a 6-inch retractable <br /> septum and the plunger actuated several times. Each vapor screen to the desired sample depth. Release the <br /> syringe should be purged of three syringe volumes before sample screen cover from the screen and retract the rod 6- <br /> collecting the sample. On the fourth purge, the plunger is inches. Place a dry bentonite powder layer in the annulus to <br /> extracted slowly until the syringe is filled with a gas sample, seal the borehole from surface air interference. Tamp the <br /> then the syringe is withdrawn and the needle immediately bentonite powder, place a hydrated bentonite layer in the <br /> plugged with a silicone stopper. The sample should be annulus, and follow with a second dry bentonite layer. Attach <br /> placed in a non-refrigerated, dry cooler with sufficient the soil gas sampling diaphragm pump to the rod casing <br /> packing to eliminate breakage during transport. Cooling using polyethylene tubing. <br /> samples will cause condensation of moisture, thereby <br /> distorting laboratory analysis. The sampling equipment consists of a TedlarTm bag <br /> (available in 1, 3, 5, and 10 liter sizes), a diaphragm pump, <br /> Duplicate air samples should be collected as in SOP-10. and 3/16-inch-diameter polyethylene tubing (approximately 1 <br /> Vapor samples are also subject to the same hold times and foot long). The TedlarTm bag should be fitted with an integral <br /> must be stored as stated in SOP-10. valve for filling and sealing the bag after sampling. The <br /> diaphragm pump inlet and outlet are fitted with 3/16-inch <br /> SOP-14 hose barbs for attaching the sample tubing. A sample label <br /> SOIL VAPOR SURVEY SAMPLING: "TEDLAR" BAG with the sample number and date and time of sample <br /> SAMPLING TECHNIQUE collection is prepared and placed on the TedlarTm bag. <br /> The sampling equipment consists of a"Tedlar" bag The sampling procedure requires one end of the tubing be <br /> (available in 1, 3, 5, and 10 liter sizes), an SKC universal slipped over the direct push drill rod sample port hose barb <br /> sample pump, soil vapor probe, and 1/4-inch-diameter and the other end over the diaphragm pump inlet hose barb <br /> polyethylene tubing (approximately three feet long). to form an air-tight connection. The sampling pump is then <br /> started and the pump is purged for 1 minute with the vapor <br /> A Roto-hammer or slam bar is used to obtain a three foot to be sampled. Following purging, the discharge of the <br /> hole into the ground area, where the soil vapor sample will pump is then connected to the TedlarTm bag using a section <br /> be collected. Once the hole has been formed the soil vapor of 3/16-inch tubing. The pump is restarted and the bag is <br /> probe will be inserted into the hole and advanced the opened and allowed to fill to approximately 3/4 of its <br /> remaining two feet, five feet total below ground surface capacity. Caution should be taken not to overfill the <br /> (bgs), with the use of either a slide hammer, using a tee sampling bag. The sample is placed in a non-refrigerated <br /> adapter and using physical force. Once the vapor probe has dry cooler with sufficient packing to prevent damage during <br />