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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> httl)//www mccampbell com E-mail main@mccampbell cam <br /> Advanced GeoEnvironmental Client Project ID Flag City Date Sampled 03/27-03128/02 <br /> 837 Shaw Road Date Received 03/28/02 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 03/28/02 <br /> Client P O Date Analyzed 03/28-04/01/02 <br /> Semi-Volatile Organics By GUMS <br /> EPA method 625 and 3510 or 8270 and 3550 <br /> Lab ID 0203513-035 <br /> Client ID EFFLUENT <br /> Matrix W <br /> Compound Concentration* An <br /> LimitCompound oncentration Report'ng Limn <br /> W S <br /> Acenaphthene ND Di-n-octyl Phthalate ND l0 033 <br /> Acenaphthylene ND 1,2-Diphenylhydrazine ND 10 033 <br /> Anthracene ND Fluoranthene ND 10 033 <br /> Benzidine ND Fluorene ND 10 033 <br /> Benzoic Acid ND 50 16 Hexachlorobenzene ND 10 033 <br /> Benzo(a)anthracene ND 10 033 Hexachlorobutadtene ND 10 033 <br /> Benzo(b)tluoranthene ND 10 033 Hexachlorocyclopentadiene ND 50 16 <br /> Benzo(k)fluoranthene ND 10 033 14exachloroethane ND 10 033 <br /> Benzo(g,h,i)perylcne ND to 033 1ndeno(1,2,3-cd)pyrene ND 10 033 <br /> Benzo(a)pyrene ND io 033 Isophorone ND 10 033 <br /> Benzyl Alcohol ND 20 066 2-Methylnaphthalene ND 10 033 <br /> • Bis(2-chloroethoxy)inethane ND 10 033 2-Methylphenol(o-Cresol) ND 10 033 <br /> Bis(2-chloroethyl)Ether ND l0 033 3&/or 4-Methylphenol(m&/or p-Cresol) ND 10 033 <br /> Bis(2-chloroisopropyl) ther ND 10 033 Naphthalene ND 10 033 <br /> Bis(2-ethylhexyl)Phthalate ND 10 033 2-Nitroanilme ND 50 16 <br /> 4-Bromophenyl Phenyl Ether ND 10 033 3-Nitroamlme ND 50 1 6 <br /> Butylbenzyl Phthalate ND 10 033 4-Nitroanilme ND 50 16 <br /> 4-Chloroanaline ND 20 066 2-Nitrophenol ND 50 16 <br /> 4-Cliloro-3-methylpheno ND 10 033 4-Nitrophenol ND 56 1 6 <br /> 2-Cliloronaphthalene ND 10 033 Nitrobenzene ND 10 033 <br /> 2-Chlorophenol ND 10 033 N-Nitrosodimethylamme ND 10 033 <br /> 4-Chlorophenyl Phenyl Ether ND 10 033 N-Nitrosodiphenylamme ND 10 033 <br /> Chrysene ND 10 033 N-Nitrosodi-n-propylamine ND 10 033 <br /> Dibenzo(a h)anthracene ND 10 033 Pentachlorophenol ND 50 16 <br /> Dibenzoturan ND 10 033 Phenanthrene ND 10 033 <br /> Di-n-butyl Phthalate ND 10 033 Phenol ND 10 033 <br /> 1 2-Dichlorobenzene ND 10 033 Pyrene ND 10 033 <br /> 1,3-Dichlorobenzene ND 10 033 1,2,4-Tnchlorobenzene ND 10 033 <br /> 1 4-Dichlorobenzene ND 10 033 2,4,5-Trichlorophenol ND 10 033 <br /> 3,3-Dichlorobenzidrne ND 20 0 66 2,4,6-Trichlorophenol ND 10 033 <br /> 2,4-Dichlorophenol ND 10 0 33 Comments <br /> Diethyl Phthalate ND t0 0 33 Surrogate Recoveries(%) <br /> 2 4-Dimethylphenol ND 10 0 33 2-Fluorophenol 42 <br /> Dimethyl Phthalate ND 10 0 33 Phenoi-d5 40 <br /> 4 6-Dinitro-2-methylphenol ND 50 1 6 Nitrobenzene-d5 55 <br /> 2 4-Dimtropheno] ND 50 16 2-Fluorobiphenyl 59 <br /> 2,4-Dtnitrotoluene ND 10 033 2,4,6-Tnbromophenoi 53 <br /> 2,6-Dtnitrotoluene ND l0 033 p-Terphenyl-d14 63 <br /> *water samples are reported in ug/L,soil and sludge samples in mg/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> • A surrogate diluted out of range <br /> h)lighter than water immiscible sheen is present,i)liquid sample that contains greate than—5 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Dizector <br />