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<br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> a//www mccampbell cam E-mail matn@mccampbell corn
<br />' Date Sampled 02/14/01 I
<br /> Advanced GeoEnvtronmental Client Project TD K& S Gas&Grocery I
<br />' 837 Shaw Road
<br /> Date Received 02/20/01
<br /> Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 02/21-02/28/01 i
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<br /> Client P O Date Analyzed 02/21-02/28/01
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 60454
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<br /> Client ID P-1/82
<br /> Matrix W
<br /> 'Repo-ung Lama Aepomng Umt
<br />' Compound Concentration* W S Compound Concentration* W S
<br /> Acetone(b) ND<20 5 0 25 trans-43-Dichloropropene ND<10 1 0 so
<br /> Benzene 350 1 0 50 Ethylene dibromide ND<10 10 5 0
<br /> Bromobenzene ND<10 1 0 5 0 Ethylbenzene 48 10 5 0
<br />' Bromochloromethane ND<10 1 0 50 14exachlorobutadiene NLK10 5 0 25
<br /> Bromodichloromethane ND<10 1 0 50 lodomethane I NLK10 10 50
<br /> Bromoform ND<10 1 0 50 Isopropylbenzene i ND<10 10 5 0
<br />' Bromomethane ND<10 1 0 5 0 p-Isopropyl toluene NLKI O 10 50
<br /> n-Butyl benzene ND<10 1 0 50 Methyl butyl ketone ND<10 10 5 0
<br /> sec-Butyl benzene ND<10 1 0 5 0 Methylene Chloride° ND<10 10 50
<br /> tort-Butyl benzene ND<10 1 0 5 0 Methyl ethyl ketone ND<10 2 0 10
<br /> Carbon Disulfide ND<10 10 50 Methyl isobutyl ketones ND<10 10 50
<br /> Carbon Tetrachloride ND<10 10 50 Methyl tert-Butyl Ether(MTBE) 10 50
<br /> Chlorobenzene NIK10 1 0 5 0 Naphthalene ND<10 50 5 0
<br /> Chloroethane ND<10 1 0 50 n-Propyl benzene ND<10 10 5 0
<br />' 2-Chloroethyl Vinyl Ether"' ND<10 l 0 5 0 Styrene ND<10 1 0 50
<br /> Chloroform NLK10 1 0 50 1,1,1,2-Tetrach1oroethane ND<10 10 50
<br /> Chlommethane ND<10 1 0 5 0 1,1,2,2-Tetrachloroethane ND<10 10 50
<br /> 2-Chlorotoluene NLK10 1 0 5 0 Tetrachloroethene ND<10 1 0 50
<br />' 4-Chlarotoluene ND<10 1 0 5 0 Toluene 25 —To 5 0
<br /> Dibromochloromethane ND<10 10 5 0 1,2,3-Tnehlorobenzene NIK10 5 0 25
<br /> 1,2-13ibromo-3-chloropropane ND<10 20 10 1,2,4-Tnchlorobenzene ND<10 5 0 25
<br /> Dibromomethane ND<10 10 5 0 1,1,1-Tnchloroethane NV<10 10 50
<br />' 1,2-Dichlorabenzene ND<10 10 5 0 1,1,2-Trichloroethane ND<10 10 50
<br /> 1,3-Dichlorobenzene ND<10 10 5 0 Trichloroethene ND<10 10 50
<br /> 1,4-Dichlorobenzene ND<10 1 0 5 0 Tnchlorofluoromethane ND<10 1 0 5 0
<br /> Dichlorodifluoromethane ND<10 1 0 5 0 1,2,3-Tnchloropropane ND<10 16 50
<br /> 1,1-Dichloroethane ND<10 1 0 5 0 1,2,4-Tnmethylbenzene 14 10 5 0
<br /> 1,2-Dichloroethane ND<10 1 0 50 1,3,5-Tnmethylbenzene ND<10 10 5 0
<br /> 1,1-Dichloroethene ND<i0 1 0 5 0 Vinyl Acetate"I ND<10 5 0 25
<br /> cis-1,2-Dichloroethene ND<10 1 0 50 Vinyl Chloride NIK10 1 0 50
<br />' trans-1,2-Dichloroethene ND<10 10 50 Xylenes,total 44 10 5 0
<br /> 1,2-Dichloropropane ND<10 10 50 Comments
<br /> 1,3-Dichloropropane ND<10 1 0 5 0 Surrogate Recoveries(%)
<br /> 2 2-Dichloropropane ND<10 1 0 5 0 Dibromofluoromethane 118
<br /> 1,1-Dichloropropene ND<10 10 50 Toluene-d8 102
<br /> 71s-1,3-Dtahloropropenc ND<IO 10 50 4-Bromofluorobenzene 98
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPL,P extracts in ug/L.
<br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) cthene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone,(h)lighter than water immiscible sheen is present, (t)liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene (o)dimethylbenzenes
<br /> DHS Certtftcation No 1644 Edward Hamilton,Lab Director
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