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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//www mccampbell_com E-mail main@mccampbell com
<br /> Advanced GeoEnvironmental Client Protect TD K& S Gas&Grocery Date Sampled 02/14/01
<br /> 837 Shaw Road Date Received 02/20/01
<br />! Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 02/21-02/28/01
<br /> I
<br /> Client P 0 Date Analyzed 02/21-02/28/01
<br />! Volatile Organics By GC/MS
<br /> EPA method 8260
<br />! Lab ID 60455
<br /> Client ID P-1195
<br /> Matnx—I W
<br /> Reporting Lime[ Repcmng Lnmt
<br />!
<br /> Compound Concentration* W S Compound Concentration* W S
<br /> Acetone chi NO 50 25 trans-1,3-Dichloropropene NO 1 0 50
<br /> Benzene 14 1 0 50 Ethylene dibromide NO l 0 50
<br />! Bromobenzene NO 1 0 50 Ethylbenzene 20 10 50
<br /> Bromochloromethane NO 1 0 50 Hexachlorobutadiene NO 50 25
<br /> Bromodichloromethane ND 10 50 lodomethane ND 10 50
<br /> Bromoform NO 10 50 Isopropylbenzene NO 10 50
<br />! Brornomethane NO 1 0 5 0 p-Isopropyl toluene NO 10 50
<br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone MNO 10 50
<br /> sec-Butyl benzene NO 1 0 50 Methylene Chloride"' NO 1 0 50
<br /> tert-Butyl benzene NO 1 0 50 Methyl ethyl ketone ND 20 10
<br /> Carbon Disulfide NO l 0 50 Methyl isobutyl ketones NO 10 so
<br /> Carbon Tetrachloride NO 1 0 50 Methyl tert-Butyl Ether(MTBE) 10 50
<br /> Chlorobenzene NO 1 0 50 Naphthalene NO 50 so
<br /> Chloroethane NO 1 0 50 n-Propyl benzene NO 1 0 50
<br />! 2-Chloroethyl Vinyl hthNO 1 0 50 Styrene NO 1 0 50
<br /> Chloroform NO 1 0 50 1,1,1,2-Tetrachloroethane ND 1 0 50
<br /> Chloromethane NO 1 0 50 1,1,2,2-Tetrachloroethane NO 1 0 50
<br /> 2-Chlorotoiuene ND 1 0 50 Tctrachloroethene ND 1 0 50
<br /> 4-Chlorotoluenc ND 10 50 Toluene 56 1 1 0 1 50
<br /> Dibromochloromethane NO 1 0 50 1,2,3-Tnchlorobenzene NO 50 25
<br /> 1,2-Dibromo-3-chloropropane NO 20 10 1,2,4-Tnchloroberizene NO 50 25
<br /> Dibromomethane NO 1 0 50 1,1,1-Tnchloroethane ND 10 50
<br /> 1,2-Dichlorobenzene NO 1 0 50 1,1,2-Tnchloroethane NO 1 0 50
<br /> 1,3-Dichlorobenzene NO 1 0 50 Tnchioroethene NO 1 0 50
<br /> 1,4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane NO 1 0 50
<br /> Dichlorodifluoromethane NO 1 0 50 1,2,3-Tnchloropropane ND 1 0 50
<br /> I 1,1-Dichloroethane ND 1 0 50 12,4-Tnmethylbenzene 26 1 0 50
<br /> 1,2-Dehloroethane 1 3 1 0 50 1,3,5-Tnmethylbenzene NO 1 0 50
<br /> 1,1-Dichloroethene NO 1 0 50 Vinyl Acetate"' NO 50 25
<br /> cis-12-Dichloroetbene ND 1 0 50 Vinyi Chloride " NO 1 0 50
<br /> trans-1,2-Dichloroethene ND to 50 Xylenes,total 8 1 1 0 50
<br /> 1,2-Dichloropropane NO 1 0 50 Comments
<br /> 1,3-Dichloropropane NO 1 0 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 119
<br /> 1,1-Dichloropropene ND 1 0 50 Toluene d8 — 102
<br /> cis-1,3-Dichloropropene ND l 0 5 0 4-Brom Aluorobenzene 98
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and al]TCLP/SPLP extracts in ug/L
<br /> I ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichioromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water mimiscible sheen is present, (i)liquid sample that contains greater than --5 vol %
<br /> sediment (1) sample diluted due to high organic content, (k) ethenylbenzene, Q) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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