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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-I620 Fax 925-798-1622 <br /> http 1/www mccampbell co m E-mail matn@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID K& S Gas&Grocery I i <br /> Date Sampled 02/14/01 <br /> 837 Shaw Road Date Received 02/20/01 <br />' Stockton, CA 95215 Client Contact Calvin Lee ' Date Extracted 02/20/01 <br /> Client P D Date Analyzed 02121-02/28101 <br />' Volatile Organics By GCIMS <br /> EPA method 8260 <br />' Lab ID 60456 <br /> Client ID P-1173-74 <br /> Matrix S <br /> Rcpvrnng Uent Reporting Limn <br />' Compound Concentration* W S Compound Concentration* W S <br /> Acetone f ND 50 25 trans-l,3-Dichlompropene ND 1 0 5 0 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 5 0 <br /> Bromobenzene ND 1 0 5 0 Ethylbenzene ND 10 50 <br />' Bromochloromethane ND 1 0 50 Hexachlorabutadiene ND 5 0 25 <br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 10 50 <br /> Bromoform ND 1 0 50 Isopropylbenzene ND 10 5 0 <br />' Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 5 0 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chlonde` ND 10 5 0 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 1 0 50 Methyl isabutyl ketone ND 10 5 0 <br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tent-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene ND 10 5 0 Naphthalene ND 5 0 5 0 <br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 10 5 0 <br />' 2-Chloroethyl Vinyl Ethe ND 10 5 0 Styrene ND 10 5 0 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND t0 50 <br /> Chloromethane ND 10 750 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chlorotoluene ND 1 0 5 0 F1,2h <br /> hloroetherre ND to 5 0 <br />' 4-Chlorotoluene ND 10 5 0 e ND 10 5 0 <br /> Dibromochloromethane ND 10 5 0 nchlorobenzene ND 50 25 <br /> 1,2-Dihromo-3-chloropropane ND 2 0 10 nchlorobenzene ND 50 25 <br /> Dibromomethane ND 10 50 1,1,1 ND 10 50 <br />' 7,2-Dichlorobenzene ND 10 5 0 Trichloroethane ND 10 5 0 <br /> 1 3-Dichlorobenzene ND 10 50 oroethene ND l p 5 0 <br /> 1,4-Dichlorobenzene ND 10 5 0 orofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 1 0 5 0 Tnchloropropane ND 1 0 5 0 <br /> I,1-Dichloroethane ND 1 0 5 0 Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 10 50 , , Tnmethylbenzene ND 10 50 <br /> 1,1-Dichloroethene ND 10 5 0 Vinyl Acetate m ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride ° ND 10 5 0 <br />' trans-1,2-Dichloroethene ND 1 0 50 Xylenes,total ND 10 50 <br /> 1,2-Dichloropropane ND 1 0 5 0 Comments <br /> 1 3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 112 <br />' 1,1-Dichloropropene ND —10 S 0 Toluene-d8 110 <br /> as-1 3-Dichloropropene ND 1 0 5 0 4-Bromofluorobenzene 113 <br /> 'water and vapor samples are reported in ug/L soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit NIA means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone (c) (2-chlotoethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacatone, (h)lighter than water immiscible sheen rs present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, ]) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />