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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//wwwmccampbellcom E-mail mann@mccampbell com
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<br /> Advanced GeoEnvironmental Client Project ID K&S Gas&Grocery Date Sampled 02/I4/O1
<br /> 837 Shaw Road Date Received 02/20/01
<br /> Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 02/21-02/28101
<br /> Client P O Date Analyzed 02121-02128101
<br /> IVolatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 60457
<br /> Client ID P-2/65'
<br /> Matrix W
<br /> Reporting Limit Reporting Limit
<br /> Compound Concentration* W S Compound Concentration* W S
<br /> Acetone roI ND 50 25 trans-1,3-Dichloropropene ND 10 50
<br /> Benzene 38 10 50 Ethylene dibromide ND 10 50
<br /> Bromobenzene ND 10 50 Ethylbenzene ND 10 50
<br /> Bromochloromethane ND 10 50 Hexachlorobutadiene ND 50 25
<br /> Bromadichloromethane ND 10 50 lodomethane ND 10 5 0
<br /> Bromoform ND 10 50 Isopropylbenzene 1 5 10 5 0
<br /> Bromomethane ND 10 50 p-Isopropyl toluene ND 10 50
<br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 10 5 0
<br /> sec-Butyl benzene ND 10 50 Methylene Cbloride` ND 1 0 5 0
<br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 10 :10 Methyl rs,,butyl ketones ND 10 5 0
<br /> Carbon Tetrachloride ND to 50 Methyl tent-Butyl Ether(MTBE) 1 0 50
<br /> Chlorobenzene ND 1 0 50 VNaphthalene ND 5 0 5 0
<br /> Chloroethane ND 1 0 50 zene ND 10 5 0
<br /> 2-Chloroethyl Vinyl Eth ND 10 50 ND 10 50
<br /> Chloroform ND 1 0 5 0 achloroethane ND 10 50
<br /> Chloromethane ND 10 50 achloroethane ND 10 5 0
<br /> 2-Chlorotoluene ND 1 0 5 0 thene ND 10 50
<br /> I 4-Chlorotoluene ND 10 50 Toluene ND 10 5 0
<br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 50 25
<br /> 12-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tncblorobenzene ND 5 0 25
<br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 10 5 0
<br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Tnehioroethane ND 10 50
<br /> 1,3-Dichlorobenzene ND 10 5 0 Tnehloroethene ND 10 5 0
<br /> 1,4-Dichlorobenzene ND 10 50 Tnchiorofluoromethane ND 10 5 0
<br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnchloropropane ND 10 50
<br /> IJ-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50
<br /> 12-Dichloroethane 1 2 to 5 0 1,3,5-Tnmethylbenzene ND 10 5 0
<br /> 1,1-Dichloroethene ND to 5 0 Vinyl Acetate irND 50 25
<br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chloride ° ND 10 50
<br /> trans-1,2-Dichloroethene ND 10 5 0 Xylenes,total ND 10 50
<br /> 1,2-Dichloropropane ND 10 50 Comments
<br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%)
<br /> 2,2-Dich1oropropane ND 10 50 Dibromolluoromethane 117
<br /> 1,I-Dichloropropene ND10 50 Toluene-d8 100
<br /> cis-1,3-Dichloropropene ND t o S 0 4-Bramofluorobenzene 100
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/1.
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, ) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamrlton,Lab Director
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