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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
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<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http/1wwwmccgLnpbcl1com E-mail main@mccarnpbell com
<br /> Advanced GeoEnvironmental Client Project ID K&S Gas&Grocery Date Sampled 02/14/01
<br /> 837 Shaw Road Date Received 02/20/01
<br /> IStockton, CA 95215 Client Contact Calvin Lee Date Extracted 02/21-02/28/01
<br /> Client P O Date Analyzed 02/21-02f28/01
<br /> Volatile Organics By GC/MS —
<br /> EPA method 8260 _
<br /> Lab ID � 60458
<br /> Client ID P-2181'
<br /> Matrix W
<br /> Compound Concentration* Repwmg iamit Compound Concentration* Rung Limit
<br />' A ____ __ W S W S
<br /> cetone Lai ND 50 25 trans-1 3-Dichloropropene ND 10 50
<br /> Benzene 61 1 0 50 Ethylene dibrorrude ND 10 50
<br /> Bromobenzene ND 1 0 5 0 Ethylbenzene ND 1 0 5 0
<br /> I Bromachloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25
<br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 10 5 0
<br /> Bromoform ND 1 0 1 5 0 lsopropylbenzene ND 1 0 5 0
<br /> I Bromomethme ND 10 5 0 p-Isopropyl toluene ND 1 0 50
<br /> n-Butyl benzene ND 10 5 0 Methyl butyl ketone ND 10 50
<br /> sec-Butyl benzene ND 10 5 0 Methylene Chloride"' ND 10 5 0
<br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone g ND 10 5 0
<br /> Carbon Tetrachlonde ND to 50 Methyl tent-Butyl Ether(MTBE) 10 5 0
<br /> Cblorobenzene ND 10 50 Naphthalene ND 50 5 0
<br /> Chloroethane ND 10 50 n-Propyl benzene ND 10 5 0
<br />' 2-Chloroethyl Vinyl Ether" ND 10 50 Styrene ND 10 5 0
<br /> Chloroform ND 10 5 0 1,1,1,2-Tetrachloroethane ND 10 5 0
<br /> Chloromethane ND 10 5 0 1,1,2,2-Tetrachioroethanc ND 10 5 0
<br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 10 50
<br />' 4-Chlorotoluene ND 1 0 50 Toluene ND 10 50
<br /> Dibroniochloromethane ND 10 5 0 1,2,3-Trichlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropme ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25
<br /> Dibromomethane ND 10 5 0 1,1,1-Tnchloroethane ND 10 50
<br /> I 1,2-Dichlorobenzene ND 1 0 5 0 1,1,2-Tnchloroethane ND 10 5 0
<br /> 1,3-Dichlorobenzene ND 1 0 5 0 Trichloroethene ND 10 5 0
<br /> 1,4-Dichlorobenzene ND 1 0 5 0 Tnehlorofluorornethane ND 1 0 5 0
<br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Tnehloropropane ND 10 50
<br />' 1,1-Dichloroethane ND 1 0 5 0 1,2,4-Tnmethylbenzene ND 10 50
<br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Tnmethylbmzene ND 10 5 0
<br /> 1,1-Dichloroethene ND 1 0 50 Vinyl Acetate m ND 5 0 25
<br /> cis-1,2-Dichlomethene ND 1 0 50 Vinyl Chloride ND 10 5 0
<br />' trans-1,2-Dichloroethene ND 1 0 50 Xylenes,total ND 10 5 0
<br /> 12-Dichloropropane ND 1 0 50 Comments
<br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 117
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<br /> 1,1-Dichlaropropene ND 10 50 Toluene-d8 103
<br /> cis-1,3-Dichloropropene ND 10 50 4-Bromofluorobenzene 100
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hezanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol %
<br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene, p) methylbenzene, (m) acetic acid ethenyl ester (n)
<br /> ehlorcethene,(0)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton, Lab Director
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