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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> AJ h l/www mccam bell com E-mail mmn@mccampbell com
<br /> Advanced GeoEnvironmental Client Protect ID K&5 Gas&Grocery I Date Sampled 02/14/01
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<br /> 837 Shaw Road Date Received 02/20/01
<br /> Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 02121-02/28/01
<br /> Client P O Date Analyzed 02121-02/28/01
<br />' Volatile Organics By GUMS
<br /> EPA method 8260 _
<br /> Lab ID 60464
<br />' Client ID P-3/95-97'
<br /> Matrix W
<br /> Compound Concentration* Rapaung Limit Compound Concentration* iteporung Limit
<br /> I W S W S
<br /> Acetone ND 50 25 trans-1,3-Dichloropropene ND 10 50
<br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 50
<br /> Bromobenzenc ND 1 0 50 Ethylbenzene ND 10 50
<br />' Bromochlorornethane ND 10 50 Hexachlorobutadiene ND 50 25
<br /> Bromodichloromethane ND 10 50 Iodomethanc ND 10 50
<br /> Bromofonn ND 10 50 Isopropylbenzene ND 10 50
<br /> Bromomethane ND 10 50 p-Isopropyl toluene ND to 50
<br />' n-Butyl benzene ND 10 50 Methyl butyl ketone ND 10 50
<br /> sec-Butyl benzene ND 10 so Methylene Chlonde° ND to 5 0
<br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone W ND 2 0 10
<br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone a ND 10 50
<br /> Carbon Tetrachlondc ND 10 50 Methyl tert-Butyl Ether(MTBE) 10 50
<br /> Chlorobenzene ND 1 0 50 Naphthalene ND 5 0 50
<br /> Chloroethane ND 1 0 5 0 n-Propyl benzene ND 10 so
<br />' 2-Chloroethyl Vinyl 8the ND 1 0 5 0 Styrene ND 1 0 50
<br /> Chloroform ND 1 0 50 1,1,1,2-Tetrachloroethane ND 1 0 5 0
<br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 1 0 5 0
<br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 1 0 5 0
<br /> 4-Chlorotoluene ND 1 0 50 Toluene ND 1 0 50
<br /> Dlbromochloromethane ND 1 0 50 1,2,3-Trichlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Trichlorobenzene ND 5 0 25
<br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 1 0 50
<br /> 1,2-Dichlorobenzene ND 1 0 50 1,1,2-Tnchloroethane ND 10 50
<br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 1 0 50
<br /> 1 4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 1 0 5 0
<br /> Dichlotodifluoromethane ND 1 0 5 0 1,2,3-Tnchloropropane ND 1 0 50
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<br /> IJ-Dichloroethane ND 1 0 5 0 1,2,4-Tnmethylbenzene ND 1 0 5 0
<br /> 1,2-achloroethane ND 1 0 5 0 L-Tnmethylbenzene ND 10 5 0
<br /> I I-Dichloroethene ND 1 0 5 0 Acetate m ND 50 25
<br /> cis-1,2-Dichloroethene ND 1 0 50 Chloride ND 10 5 0
<br /> trans-l,2-Dichloroethene ND 1 0 5 0 nes,totalND 10 50
<br /> l,2-Dichloropropane ND 1 0 50 ments
<br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane N ND 1 0 50 Dibromofluoromethane 118
<br />' 1,1-Dichloropropene ND l0 50 Toluene-dS 105
<br /> cis-1,3-I)ichloropropene ND l 0 5 0 4 Bromofluorobenzene 101
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I SPLP extracts in ug/L
<br /> ND means not detected above the reporting Brut,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present, (1)liquid sample that contains greater than --5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, } methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton, Lab Director
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