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<br /> 110 2nd Avenue South,#137,Pacheco,CA 94553-5560
<br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http-//www mccampbell com E-mail main@mecampbell coin
<br />' Advanced GeoEnvironmental Client Protect ID K&S Gas&Grocery Date Sampled 02/14/01
<br /> 837 Shaw Road , Date Received 02/20/01
<br />' Stockton, CA 952I5 Client Contact Calvin Lee Date Extracted 02121-02/28101
<br />' Client P O Date Analyzed 02/21-02128101
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br />' Lab ID 60465
<br /> Client ID P-3/117-121'
<br /> Matnx W
<br /> Reporting Umit Re
<br /> porung Limn
<br />' Compound Concentration* W S Compound Concentration* W S
<br /> Acetone mi ND<50 50 25 trans-1,3-Dichloropropene ND<5 0 1 0 5 0
<br /> Benzene 270 1 0 50 Ethylene dibromide ND<5 0 1 0 5 0
<br />' Bromobenzene ND<5 0 10 50 Ethylbenzene ND<5 0 1 0 5 o
<br /> Bromochlotornethane ND<5 0 10 50 Rexachlorobutadiene ND<5 0 5 0 25
<br /> Bromodichloromethane ND<5 0 10 50 lodomethane NI3<5 0 1 0 5 0
<br /> Bromoform ND<5 0 10 50 Isopropylbenzene ND<5 0 10 50
<br />' Bromomethane ND<5 0 1 0 50 p-Isopropyl toluene NIX5 0 10 50
<br /> n-Butyl benzene ND<5 0 1 0 50 Methyl butyl ketone ND<5 0 1 0 50
<br /> sec-Butyl benzene ND<5 0 1 0 50 Methylene Chloride` ND<15 10 50
<br /> tert-Butyl benzene ND<5 0 1 0 50 Methyl ethyl ketone ND<5 0 20 10
<br /> Carbon Disulfide ND<5 0 1 0 50 Methyl isobutyl ketone ND<5 0 10 50
<br /> Carbon Tetrachloride ND<5 0 1 0 5 0 Methyl tert-Butyl Ether(MTBE) 10 50
<br /> Chloroberizene ND<5 0 1 0 50 Naphthalene ND<5 0 50 50
<br /> Chloroethane ND<5 0 10 50 n-Propyl benzene ND<5 0 10 5 0
<br />' 2-Chloroethyl Vinyl Ether"' ND<5 0 10 50 Styrene ND<5 0 10 5 0
<br /> Chloroform ND<5 0 1 0 5 0 1,1,1,2-Tetrachloroethane ND<5 0 10 5 0
<br /> Chloromethane ND<5 0 1 0 50 1,1,2,2-Tetrachloroethane ND<5 0 10 5 0
<br /> 2-Chlorotoluene ND<5 0 1 0 50 Tetrachloroethene ND<5 0 10 5 0
<br /> 4-Chlorotoluene ND<5 0 1 0 50 Toluene M 6 4 10 5 0
<br /> Dibromochloromethane ND<5 0 l 0 50 1 2 3-Tnchlorobenzene ND<5 0 5 0 25
<br /> 1,2-Dibromo-3-chloropropanc ND<5 0 2 0 10 1,2,4-Tnchlorobenzene ND<5 0 50 25
<br /> Dibromomethane ND<5 0 10 50 1,1,1-Tnehloroethane ND<5 0 10 5 0
<br /> I 1,2-Dichlorobenzene ND<5 0 1 0 5 0 1,1,2-Trichloroethane ND<5 0 10 50
<br /> l,3-Dich1orobenzene ND<5 0 1 0 50 Trichloroethene ND<5 0 1 10 5 0
<br /> 1,4-Dichlorobenzene ND<S 0 1 0 5 0 Tnehlorofluoromethane ND<5 0 10 50
<br /> Dichlorodifluoromethane ND<5 0 1 0 5 0 1,2,3-Tnehloropropane ND<5 0 10 50
<br />' 1,1-Dichloroethane ND<5 0 1 0 5 0 1,2,4-Tnmethylbenzene ND<5 0 to 50
<br /> 1,2-Dichloroethane ND<5 0 1 0 5 0 1,3,5-Tnmethylbenzene ND<5 0 10 5 0
<br /> 1,1-Dichloroethene ND<5 0 1 0 5 0 Vinyl Acetate °' ND<5 0 5 0 25
<br /> cis-1,2-Dichloroethene ND<5 0 1 0 5 0 Vinyl Chloride " ND<5 0 to 50
<br />' trans-1,2-Dichloroethene ND<5 0 1 0 5 0 Xylenes,total 5 1 10 5 0
<br /> 1,2-Dichloropropane ND<5 0 1 0 5 0 Comments
<br /> 1,3-Dichloropropane ND<5 0 1 0 5 4 Surrogate Recoveries
<br /> 2,2-Dichloropropane ND<5 0 1 0 5 0 Dibromotluoromethane 117
<br /> 1,1-Dichloropropene ND<5 0 1 0 5 0 Toluene-d8 102
<br /> cis-1,3-Dichloropropane ND<5 0 1 0 5 0 4-Bromofluorobenzene 121
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in uglkg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c)(2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2-
<br /> Pentatione or isopropylaectone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than ---5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hanulton,Lab Director
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