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I <br /> 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL .ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwmccarnpbellcom E-mail team@mccampbell corn <br />' Advanced GeoEnvtronmental Client Project ID K& S Gas&Grocery Date Sampled 02/14/01 j <br /> 837 Shaw Road ; Date Received 02/20/01 <br /> fStockton, CA 95215 Client Contact Calvin Lee Date Extracted 02/21-02/28/01 <br /> Client P O Date Analyzed 02/21-02/28/01 <br />' 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> I Lab ID 60453 60454 60455 60456 <br /> Reporting Limit <br /> Client ID P-1/65 P-1/82 P-1/95 P-1173-74 <br />' Matrix W W W S S w <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND<10 ND<10 ND ND 50 1 0 <br />' Ethyl tert-Butyl Ether(ETBE) ND<10 ND<10 ND ND so 1 0 <br /> Methyl-tert Butyl Ether(MTBE) ND<10 ND<10 ND ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND<10 ND<10 ND ND 50 10 <br /> tert-Butanol N13<50 ND<50 ND ND 25 50 <br /> IMethanol ND<2000 ND<2000 ND ND 1000 200 <br /> Ethanol ND<500 ND<500 ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromotluoromethane 114 118 119 H2 <br /> Comments J 1 <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment 0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />