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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell com E-mail main@mccampbelI corn <br /> Advanced GeoEnvironmental Client Project ID K& S Gas&Grocery Date Sampled 02/14/01 <br /> 837 Shaw Road Date Received 02/20/01 <br />' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 02/2I-02/28101 <br /> -- Client P O Date Analyzed 02/21-02/28/01 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 60457 60458 60459 60460 <br /> Reporting Limit <br /> Client ID P-2165' P-2/8I' P-2/93' P-2/7I-72' <br /> Matnx W W W A S 5 W <br /> Compound Concentration* uglkg ug/L <br /> Di-isopropyl Ether(DfiPE) 20 ND ND ND so 1 0 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND ND 50 10 <br /> tert-Amyt Methyl Ether(TAME) ND ND ND ND 50 10 <br /> tert-Butanol ND 5 0 ND ND 2550 <br /> Methanol ND ND ND ND 1000 200 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries <br /> Dibromofluoromethane 117 117 119 111 <br />' Comments <br /> 11 N <br /> water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />