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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 h9p://www.mccampbell.com E-mail:main@mecampbell.com Advanced GcoEnviromnental Client Project-ID- Hess Du Bois Date.Sampled: 04118-04/19/01 837 Shaw Road Date Received: 04/23/01 ' Stockton, CA 95215 Client Contact: Bill Little Date Extracted: 04/23/01 ' Client P.O: Date Analyzed: 04/23-04126/01 Volatile Organics By GUMS EPA method 8260 ' Lab ID 65985 Client ID MW9-20 Matrix S Reporting Limit Reporting Limit ' Compound Concentration* W S Compound Concentration* -W S Acetone syr ND<25,000 5.0 25 trans-1,3-Dichloropropene ND<1000 LO 5.0 Benzene ND<1000 1.0 5.0 Ethylene dibromide ND<l000 1.0 5.0 Bromobenzene ND<1000 1.0 5.0 Ethylbenzene ND<1000 1.0 5.0 ' Bromochloromethane ND<1000 1.0 5.0 14exachlorobutadiene ND<1000 5,0 25 Bromodichloromethane ND<1000 1.0 5.0 lodometbane ND<1000 LO 5.0 Bromo€orm ND<1000 1.0 5.0 lsopro ylbenzene 1000 1.0 5.0 ' Bromomethane ND<1000 1.0 5.0 p-Isopropyl toluene 3400 1.0 5.0 n-Butyl benzene 4400 1.0 5.0 Methyl butyl ketone tdi ND<1000 1.0 5-0 sec-Butyl benzene 2400 1.0 5.0 Methylene Chlorides" ND<4500 L0 5.0 tert-Butyl benzene ND<1000 1.0 5.0 Methyl ethyl ketone to ND<1000 2.0 10 Carbon Disulfide ND<1000 1.0 5.0 Methyl isobutyl ketone ND<1000 1.0 5.0 Carbon Tetrachloride ND<1000 1.0 5.0 Methyl tert-Butyi Ether(MTBE) 1.0 5.0 Chlorobenzene ND<1000 1.0 5.0 Naphthalene ND<1000 5.0 5.0 Chloroethane ND<1000 1.0 5.0 n-Propyl benzene 3300 1.0 5.0 ' 2-Chloroethyl Vinyl Ether(c) ND<1000 1.0 5.0 Styrene 00 N0<1000 1.0 5.0 Chloroform ND<1000 1.0 5.0 1,1,1,2-Tetrachloroethane N13<1000 LO 5.0 Chloromethane ND<1000 1.0 5.0 1,1,2,2-Tetrachloroethane ND<1000 1.0 5.0 2-Chlorotoluene ND<1000 1.0 5.0 Tetrachloroethene ND<1000 1.0 5.01. - - 4-Chlorotoluene ND<1000 1.0 5.0 Toluene(1) ND<1000 1.0 5.0 ' Dibromochloromethane ND<1000 1.0 5.0 1,2,3-Trichlorobenzene ND<1000 5.0 25 1,2-Dibromo-3-chloropropane ND<1000 2.0 10 1,2,4-Trichlorobenzene ND<1000 5.0 25 Dibromomethane ND<1000 1.0 5.0 1,1,1-Trichloroethane ND<1000 1.0 5.0 ' 1,2-Dichlorobenzene N13<1000 1.0 5.0 1,1,2-Trichloroethane ND<1000 1.0 5-0 1,3-Dichlorobenzene ND<1000 1.0 5.0 Trichloroethene ND<1000 1.0 5.0 1,4-Dichlorobenzene N13<1000 1.0 5.0 Trichlorofluoromethane ND<1000 1.0 5.0 Dichlorodifluoromethane ND<1000 1.0 5.0 1,2,3-Trichloropropane ND<1000 1.0 5.0 ' t,l-Dichloroethane ND<1000 1.0 5.0 1,2,4-Trimeth lbenzene 10,000 1.0 5.0 1,2-Dichloroethane ND<1000 1.0 5.0 1,3,5-Trimethylbenzene 3400 1.0 5.0 I,1-Dichloroethene ND<1000 1.0 5.0 Vinyl Acetate c't ND<1000 5.0 25 cis-1,2-Dichloroethene ND<1000 1.0 5.0 Vinyl Chloride s"r ND<1000 1.0 5.0 ' trans-l,2-Dichloroethene ND<1000 1.0 5.0 Xylenes,total ND<1000 1.0 5.0 1,2-Dichlaropropane ND<1000 1.0 5.0 Comments: 1,3-Dichloro ro ane ND<1000 1.0 5.0 Surrogate Recoveries % 2,2-Dichloropropane ND<1000 1.0 5.0 Dibromofluoromethane 110 1,1-Dichloropropene. ND<1000 1.0 5.0 Toluene-d8 103 cis-1,3-Dichloro ro ene ND<1000 1.0 5.0 4-Bromofluorobenzene 87 water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L ' ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than-5 vol. % sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) chloroethene; a dimethylbenzenes. DHS Certification No. 1644 Edward Hamilton,Lab Director