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110 2nd Avenue South,#137,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//wwwmcEAMpbe1lcorn E-mail main@mccampbell corn
<br /> GEOSOLV, LLC Client Project ID Nunan/Jernigan Date Sampled 02120-03/01/01
<br /> 643 Oregon Street Date Received 03/01/01
<br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01
<br /> Client P O Date Analyzed 03/05-03/0$101
<br /> Volatile Organics By GC/MS
<br /> EPA method$260
<br /> Lab ID 61524
<br /> Client ID MW-3 23"2-24
<br /> Matrix S
<br /> Repontng Limit Reponmg Limit
<br /> Compound Concentration* W S Compound Concentration* W S
<br /> Acetone(b) Nl?<35 50 25 trans-1,3-Dichloropropene ND 10 50
<br /> Benzene ND 10 5 0 Ethylene dibromide ND 10 5 0
<br /> Bromobenzene ND 10 5 0 Ethylbenzene ND 10 5 0
<br /> Bromochloromethane ND 1 0 5 0 Hexachlorobutadiene ND 5 0 25
<br /> Bromodichloromethane ND 10 5 0 lodomethane ND 10 5 0
<br /> Bromoform ND 10 5 0 Isopropylbenzene ND 10 5 0
<br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 10 5 0
<br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 10 5 0
<br /> sec-Butyl benzene ND 1 0 50 Methylene Chlonde e ND 10 5 0
<br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketones ND 1 0 5 0
<br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) --- 1 0 50
<br /> Chlorobenzene ND 10 5 0 Naphthalene ND 5 0 50
<br /> Chloroethane ND 10 5 0 n-Propyl benzene ND 10 50
<br /> 2-Chloroethyl Vinyl Ether` ND 10 50 styrene M ND 10 5 0
<br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50
<br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 1 0 5 0
<br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 10 50
<br /> 4-Chlorotoluene ND 1 0 5 0 Toluene 21 10 50
<br /> Dibromochloromethane ND 1 0 5 0 1,2,3-Tnchlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Trichlorobenzene ND 5 0 25
<br /> Dibromomethane ND 10 50 1,1,1-Tnchloroethane ND 10 50
<br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND 10 50
<br /> 1,3-Dichlorobenzene ND 1 0 50 Tnchloroethene ND 10 5 0
<br /> 1,4-Dichlorobenzene ND 10 5 0 Tnchlorofluoromethane ND 10 1 5 0
<br /> Dichlorodift0romethane ND 10 50 1,2,3-Trichloropropane ND 10 50
<br /> 1,1-Dichloroethane ND 10 5 0 1,2,4-Trimethylbenzene 59 10 5 0
<br /> 1,2-Dichloroethane ND 10 50 1,3 5-Trimethylbenzene ND 10 50
<br /> 1,1-Dichloroethene ND 10 5 0 Vinyl Acetate(`3 ND 50 25
<br /> cis-1,2-Dtchloroethene ND 10 5 0 Vinyl Chloride ND 10 5 0
<br /> trans-1,2-Dtchloroethene ND 10 50 Xylenes,total ND 10 5 0
<br /> 1,2-Dich1oropropane ND 10 50 Comments
<br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND I 0 5 0 Dibromofluoromethane 96
<br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 102
<br /> cis-1,3-Dichloropropene ND 1 0 S 0 4-Bromofluorobenzene 96
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ughmpe and all TCLP/SPLP extracts in ug/L
<br /> ND mcans not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane (f) 2-butanone (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol %
<br /> sediment, G) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroetbene (o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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