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110 2nd Avenue South,4D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http I/www mccampbell coin E-mail main@mccampbeli com
<br /> GEOSOLV,LLC Client Project 1D Nunan/Jemigan Date Sampled 02/20-03/01/01
<br /> 643 Oregon Street Date Received 03/01/01
<br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01
<br /> Client P O Date Analyzed 03/05-03108101
<br /> Volatile Organics By GC/MS
<br /> EPA method$260
<br /> Lab ID 61525
<br /> Client ID MW-3 30"2-31
<br /> Matrix S
<br /> Reponmg Limit M, Ortmf
<br /> Limit
<br /> Compound Concentration* W S Compound Concentration* S
<br /> Acetone(d) ND<100 50 25 trans 1,3-Dichloropropene ND<100 50
<br /> Benzene 130 1 0 50 Ethylene dibromide ND<100 so
<br /> Bromobenzene ND<100 1 0 50 Ethylbenzene 1300 50
<br /> Bromochloromethane ND<100 1 0 50 Hexachlorobutadiene ND<100 25
<br /> Bromodichloromethane ND<100 1 0 50 lodomethane ND<100 50
<br /> Bromoform ND<100 1 0 50 Isopropylbenzene 220 1 0 50
<br /> Bromomethane ND<100 10 50 p4sopropyl toluene 220 10 50
<br /> n-Butyl benzene 400 1 0 50 Methyl butyl ketone ND<100 10 50
<br /> sec-Butyl benzene 200 1 0 50 Methylene Chloride"' ND<120 10 50
<br /> tert-Butyl benzene ND<100 1 0 50 Methyl ethyl ketone ND<100 20 10
<br /> Carbon Disulfide ND<100 1 0 50 Methyl isobutyl ketone 191 ND<100 10 50
<br /> Carbon Tetrachloride ND<100 1 0 50 Methyl tert-Butyl Ether(MTBE) --- 10 50
<br /> Chlorobenzene ND<100 10 50 Naphthalene ND<100 50 50
<br /> Chloroethane ND<100 10 50 n-Propyl benzene 690 10 50
<br /> 2-Chloroethyl Vinyl Ether` ND<100 10 50 Styrene M ND<100 10 50
<br /> Chloroform ND<100 1 0 50 1,1,1,2-Tetrachloroethane NIK100 1 0 50
<br /> Chloromethane ND<100 1 0 50 1 1,2,2-Tetrachloroethane ND<100 10 50
<br /> 2-Chlorotoluene ND<100 1 0 50 Tetrachloroethene ND<100 1 0 50
<br /> 4-Chlorotoluene ND<100 l 0 50 Toluene 130 10 50
<br /> Dibromochloromethane ND<100 l 0 50 1,2,3-Tnehlorobenzene ND<100 50 25
<br /> 1,2-Dibrorna-3-chloropropane ND<100 20 10 1,2,4-Tnchlorobenzene ND<I00 50 25
<br /> Dibromomethane ND<100 1 0 50 1,1,1-Tnchloreethane ND<100 10 50
<br /> 1,2-Dichlorobenzene ND<100 10 50 1,1,2-Tnchloroethane ND<100 10 50
<br /> 1,3-Dichlorobenzene NIX100 l 0 50 Trichloroethene ND<100 1 0 50
<br /> 1,4-Dichlorobenzene ND<100 l 0 50 Trichlorofluoromethane ND<100 10 50
<br /> Dtchlorodifluoromethane ND<100 1 0 50 1,2,3-Tnchloropropane ND<100 10 50
<br /> IJ-Dichloroethane ND<100 10 50 1,2,4-Tnmethylbenzene 2400 10 50
<br /> 112-Dichloroethane ND<100 1 0 50 1,3,5-Trimethylbenzene 990 10 so
<br /> I,1-Dichloroethene NLK100 10 50 VmylAcetate " ND<100 50 25
<br /> cis-1,2-Dichloroethene ND<100 10 50 Vinyl Chloride " ND<100 10 50
<br /> trans-1,2-Dichloroethene ND<100 1 0 50 Xylenes,total 1400 1 0 50
<br /> 1,2-Dichlaropropane ND<100 10 50 Comments
<br /> 1,3-Dichloropropane ND<100 1 0 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND<100 1 0 50 Dibromofluoromethane 90
<br /> 1,1-Dichloropropene ND<100 1 0 50 Toluene-0 103
<br /> cis-1,3-Dichloropropene ND<100 1 0 50 4-Bromofluorobenzene 94
<br /> water and vapor samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> . (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present (1)liquid sample that contains greater than --5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br />' chloroethene,(o)dimethylbenzenes
<br /> DHS Certif cation No 1644 Edward Hamilton, Lab Director
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