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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 http//www mccampbell com E-mail mai cr mccampbell com <br /> GEOSOLV,LLC Client Project ID Nltnan/Jemigan Date Sampled 02/20-03/01/01 <br /> 643 Oregon Street Date Received 03/01/01 <br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01 <br /> Client P O Date Analyzed 03/05-03/08/0I <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> 1 Lab ID 61526 <br /> Client ID MW-3 36-36 <br /> Matrix S <br /> Reporting Limit Reponmg Lima <br /> 1 Compound Concentration* W S Compound Concentration* W S <br /> Acetone ror ND<50 50 25 trans-l,3-Dichloropropene ND<20 10 50 <br /> Benzene 150 1 0 50 Ethylene dibromide ND<20 10 50 <br /> Bromobenzene ND<20 1 0 50 Ethylbenzene 340 10 50 <br /> Bromochloromethane ND<20 1 0 5 0 Hexachlorobutadiene ND<20 50 25 <br /> Bromodichloromethane ND<20 1 0 50 lodomethane ND<20 10 5 0 <br /> Bromofonn ND<20 1 0 50 Isopropyibenzene 26 10 50 <br />' Bromomethane ND<20 10 50 -Iso ro 1 toluene ND<20 10 50 <br /> n-Butyl benzene ND<20 1 0 50 Methyl butyl ketone cal ND<20 to 5 0 <br /> sec-Butyl benzene ND<20 1 0 5 0 Methylene Chloride(`[ ND<20 10 5 0 <br /> tert-Butyl benzene ND<20 1 0 5 0 Methyl ethyl ketone ca ND<20 2 0 10 <br /> Carbon Disulfide ND<20 1 0 50 Methyl isobutyl ketone cal ND<20 10 50 <br /> Carbon I etrachloride ND-20 1 0 50 Methyl tcn-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene ND<20 10 5 0 Naphthalene ND<20 5 0 5 0 <br /> Chloroethane ND<20 1 0 5 0 n-Propyl benzene 120 1 0 50 <br />' 2-Chloroethyl Vinyl Ethe& ND<20 1 0 5 0 Styrene"F ND<20 1 0 50 <br /> Chloroform ND<20 1 0 5 0 1,1,1,2-Tetrachloroethane ND<20 1 0 50 <br /> Chloromethane ND<20 1 0 5 0 1 1 2 2-Tetrachloroethane ND<20 1 0 50 <br /> 2-Chlorotoluene ND<20 1 0 5 0 Tetrachloroethene ND<20 1 0 50 <br /> 1 4-Chlorotoluene ND<20 1 0 5 0 Toluene ui 950 10 50 <br /> Dibromochloromethane ND<20 10 50 1 2,3-Trichlorobenzene ND<20 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND<20 20 10 1,2,4-Trichlorobenzene ND<20 5 0 25 <br /> Dibromomethane ND<20 10 5 0 1 1 I-Trichloroethane ND<20 10 50 <br /> 1,2-Dichlorobenzene ND<20 1 0 50 1,1,2-Trichloroethane ND<20 10 5 0 <br /> 1,3-Dichlorobenzene ND<20 to 50 Trichloroethene ND<20 1 0 5 0 <br /> 1,4-Dichlorobenzene ND<20 1 0 5 0 Tnchiorofluoromethane ND<20 1 0 5 0 <br /> Dichlorodifluoromethane ND<20 1 0 50 1 2 3-Tnchloropropane ND<20 10 5 0 <br /> 1 1 1-Dichloroethane ND<20 10 5 0 1,2,4-Trimethylbenzene 570 10 50 <br /> t,2-Dichloroethane ND<20 1 0 5 0 1,3,5-Trimeth (benzene 190 1 0 5 0 <br /> l,l-Dichloroethene ND<20 1 0 50 Vinyl Acetate 11 ND<20 5 0 25 <br /> cis-1,2-Dichloroethene ND<20 1 0 50 Vinyl Chloride'") ND<20 10 50 <br /> trans-1,2-Dichloroethene ND<20 1 0 5 0 Xylenes,total i°i 1500 ] 0 5 0 <br /> 42-Dichloropropane ND<20 1 0 5 0 Comments <br /> 1,3-Dichloro ro ane ND<20 1 0 5 0 Surrogate Recoveries <br /> 2,2-Dichloropropane ND<20 1 0 5 0 Dibromofluoromethane 90 <br /> 1 1,1-Dichloropropene ND<20 1 0 50 Toluene-d8 100 <br /> cis-I 3-Dichloro ro ene ND<20 1 0 50 4-Bromofluorobenzene 91 <br /> 'water and vapor samples are reported in ug/L soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (e) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester (n) <br /> chloroethene o dimeth lberizenes <br /> DHS Certification No 1644 — __Edward Hamilton, Lab Director <br />