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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC I Telephone 925-798-1620 Fax 925-798-1622
<br /> http//www mccamphell corn E-mail main@mccampbell corn
<br /> GEOSOLV,LLC Client Project ID Nunan/Jemigan Date Sampled 02120-03101/01
<br /> 643 Oregon Street Date Received 03/01/01
<br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01
<br /> Client P O Date Analyzed 03/05-03/08/01
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 61528
<br /> 1 Client ID MW-3 45 -46
<br /> Matnx S
<br /> Reporting Limit Reporting Limit
<br /> Compound Concentration* W 3 Compound Concentration* W S
<br /> 1 Acetone tb) NIX35 50 25 trans-1,3-Dichloropropene ND 1 0 50
<br /> Benzene ND 10 50 Ethylene dibromide ND 1 0 50
<br /> Bromobenzenc ND 10 50 Ethylbenzene ND 1 0 50
<br /> 1 Bromochloromethane ND 10 50 Hexachlorobutadiene ND 50 25
<br /> Bromodichloromethane ND 10 50 lodomethane ND 10 50
<br /> Bromoforin ND 10 50 isopropylbenzene ND 1 0 so
<br /> Bromomethane ND 10 50 p-Isopropyl toluene ND 1 0 50
<br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 10 50
<br /> sec-Butyl benzene ND 10 50 Methylene Chlonde"I Chloride" ND 1 0 50
<br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 20 10
<br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketones ND 1 0 5 0
<br /> Carbon Tetrachloride ND 10 50 Methyl tert-Butyl Ether(MTBE) --- 10 50
<br /> Chlorobenzene ND 10 50 Naphthalene ND 50 50
<br /> Chloroethane ND 10 50 n-Propyl benzene ND 10 5 0
<br /> 2-Chloroethyl Vinyl Ethe ND 10 50 Styrene ND 10 50
<br /> Chloroform ND 10 5 0 1,1,1 2-Tetrachloroethane ND 10 50
<br /> Chloromethane ND 1 0 5 0 1,1,2,2 Tetrachloroethane ND 10 5 0
<br /> 2-Chlorotoluene ND 10 5 0 Tetrachloroethene ND 10 5 0
<br /> 4-Chlorotoluene ND 1 0 5 0 Toluene 14 10 50
<br />' DibromochlOTOmethane ND 10 50 1 2 3-Trichlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 50 25
<br /> Dibromomethane ND 1-6 50 1 1,]-Tnchloroethane ND 10 5 0
<br /> 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Trichloroethane ND 10 5 0
<br /> 1 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 10 5 0
<br /> 1,4-Dichlorobenzene ND 10 5 0 Trichlorofluoromethane ND 10 5 0
<br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Tnehloropropane ND 1 0 5 0
<br /> I,1-Dichloroethane ND 10 5 0 1 2,4-Tnmethylbenzene ND 1 0 5 0
<br /> 1,2-Dichloroethane ND 10 5 0 1,3,5-Trimethylbenzene ND 10 5 0
<br /> LI-Dichloroethene ND 1 0 5 0 Vinyl Acetate ND 50 25
<br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride ND 1 0 5 0
<br /> trans-l,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 10 50
<br /> 1,2-Dichloropropane ND 1 0 5 0 Comments
<br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%)
<br /> 2 2-Dichloropropane ND 1 0 50 Dibromofluoromethane 97
<br />' 1,1-Dichl0r0propene I ND 10 50 Toluene-M 103
<br /> cis-1,3-Dichloropropene ND 1 0 1 5 0 4-Bromofluorobenzene 91
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2 chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (t) 2-but2nonc (g) 4-methyl-2-
<br /> pentanone or isopropyl acetone, (h)lighter than water immiscible sheen is present, (t) liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br />' chloroethene {o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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