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1102nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-7622
<br /> IF44 http l/www mccargpbell com E-mail main@mccampbell corn
<br /> 1 GEOSOLV,LLC Client Project ID Nunan/Jernigan Date Sampled 02/20-03/01/01
<br /> 643 Oregon Street Date Received 03/01/01
<br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01
<br /> Client P O Date Analyzed 03/05-03/08/01
<br /> 1Volatile Organics By GCIMS
<br /> EPA method 8260
<br /> Lab ID 61530
<br /> I Client ID MW-3 60""-61
<br /> Matrix S
<br /> Reporting Unnt Reporting Limit
<br /> Compound Concentration* W S Compound Concentration* W S
<br />' Acetone(s) ND<35 50 25 trans-1,3-Dichloropropene ND 10 50
<br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 5 0
<br /> Bromobenzene ND 1 0 50 Ethylbenzene 6 4 10 5 0
<br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25
<br /> Bromodichloromethane ND 1 0 5 0 lodomethane ND 1 0 1 5 0
<br /> Bromofonrt ND 10 50 Isopropylbenzene ND 1 0 5 0
<br /> Bromomethane ND 10 50 p-Isopropyl toluene ND 1 0 5 0
<br />' n-Butyl benzene ND 10 50 Methyl butyl ketorIC717ND 1 0 50
<br /> sec-Butyl benzene ND 1 0 50 Methylene Chi onde` ND 1 0 5 0
<br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 10 50 Methyl ncibutylketones ND 1 0 5 0
<br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) --- 10 5 0
<br /> Chlorobenzene ND 1 0 50 Naphthalene ND 5 0 50
<br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 10 5 0
<br /> 2-Cbloroethyl Vinyl Ether(') ND 1 0 5 0 Styrene MND 10 5 0
<br />' Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50
<br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 10 5 0
<br /> 2-Chlorotoluene ND 1 0 5 0 TetrachlOTOelhene ND 10 50
<br /> 4-Chloretoluene ND 1 0 5 0 Toluene 71 10 5 0
<br />' Dibromochloromethane ND 1 0 50 1,2,3-Tnchlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25
<br /> Dibromomethane ND 10 5 0 1,1,1-Trichloroethane ND 10 5 0
<br /> 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Trichloroethane ND 10 5 0
<br />' 1,3-Dichlorobenzene ND 1 0 5 0 Trichloroethene ND 1 0 5 0
<br /> 1 4-Dichlorobenzene ND 1 0 5 0 Trichlorofluoromethane ND 1 0 5 0
<br /> Diebiorodifluoromethane ND 1 0 5 0 1,2,3-Tnchloropropane ND 1 0 5 0
<br /> 1 1-Dichloroethane ND 1 0 5 0 1,2,4-Tnmethylbenzene 16 1 0 5 0
<br />' 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Trimethylbenzene 61 1 0 5 0
<br /> 1 1-Dichloroethene ND 1 0 5 0 Vinyl Acetate m ND 5 0 25
<br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride " ND 1 0 5 0
<br /> trans-1,2-Dichloroethene ND 1 0 5 0 Xylenes,total 32 1 0 5 0
<br /> 1,2-Dichloropropane ND 10 50 Comments
<br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%)
<br /> 2 2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane 96
<br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 104
<br /> cis-1,3-Dichloropropene ND 10 50 1 4-Bromofluorobenzene 91
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (c) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, ( methylbenzene, (m) acetic acid ethenyl ester (n)
<br />'
<br /> chl oroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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