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1 110 2nd Avenue South,##D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//www mccampbell com E-mail main@mccampbell com
<br /> GEOSOLV,LLC Client Project ID Nunan/Jernigan Date Sampled 02120-03/01101
<br /> 643 Oregon Street Date Received 03/01/01
<br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01
<br /> Client P O Date Analyzed 03105-03/08/01
<br />' Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 61531
<br /> Client ID MW-3 70"1-71
<br /> Matrix S
<br /> Aep°rtmg Limit Reporting Limit
<br /> Compound Concentration* W S Compound Concentration* W S
<br />' Acetone m> ND<35 50 25 trans-l,3-Dichloropropene NO 10 50
<br /> Benzene NO ] 0 5 0 Ethylene dibromide NO 10 5 0
<br /> Bromobenzene NO 1 0 5 0 Ethylbenzene NO 10 5 0
<br /> t Bromochloromethane NO 1 0 5 0 Hexachlorobutadiene NO 50 25
<br /> Bromodichloromethane NO 1 0 5 0 lodomethane NO 10 5 0
<br /> Bromoform NO 1 0 5 0 Isopropylbenzene NO 1 0 5 0
<br /> Bromomethane NO 1 0 50 p-Isopropyl toluene NO 1 0 50
<br /> dF
<br /> n-Butyl benzene NO 10 5 0 Methyl bury]ketone NO 1 0 5 0
<br /> sec-Butyl benzene NO 1 0 50 Methylene Chlunde` NO 10 5 0
<br /> tert-Butyl benzene NO 1 0 5 0 Methyl ethyl ketone NO 2 0 10
<br /> Carbon Disulfide NO 10 5 0 Methyl isobutyl ketones ND 10 5 0
<br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert Butyl Ether(MTBE) --- 10 5 0
<br /> Chlorobenzene NO 10 50 Naphthalene ND 50 5 0
<br /> Cbloroethane NO 10 5 0 n-Propyl benzene NO 10 50
<br /> 2-Chloroethyl Vinyl Ether"' NO 10 50 Styrene NO 10 50
<br /> Chloroform NO 10 5 0 1,1,1,2-Tetrachloroethane ND 10 5 0
<br /> Chloromethane NO 10 60 1,1,2,2-Tetrachloroethane NO 10 50
<br /> 2-Chloretoluene NO 10 5 0 Tetrachloroethene NO 10 5 0
<br /> 4-Chlorotoluene NO 10 50 Toluene 66 10 5 0
<br />' Dibromochloromethane NO 10 50 1,2,3-Trichlorobenzene NO 5 0 25
<br /> 1,2-Dibromo-3-chloropropane NO 20 10 1,2,4-Trichlorobenzene NO 5 0 25
<br /> Dibromomethane NO 10 50 1,1,1-Trichloroethane NO 10 50
<br /> 1,2-Dichlorobenzene NO 10 50 1,1,2-Trichloroethane NO 10 50
<br />' 1,3-Dichlorobenzene NO 10 50 Trichloroethene NO 10 50
<br /> 1,4-Dichlorobenzene NO 1 0 5 0 Trichlorofluoromethane NO 1 0 50
<br /> Dichlorodifluoromethane NO 10 50 1,2,3-Tnehloropropane NO 10 50
<br />' ],l-Dichloroethane NO 10 50 1,2,44nmethylbenzene NO 10 50
<br /> 1,2-Dichloroethane NO 1 0 5 0 1,3,5-Tnmethylbenzene NO to 50
<br /> I,1-Dich1oroethene NO 1 0 5 0 Vinyl Acetate'ral ND S Q 25
<br /> cis-1,2-Dichloroethene NO 10 50 Vinyl Chlonde " ND 10 5 0
<br /> trans-l,2-Dichloroethene NO 10 5 0 Xylenes,total ND 10 50
<br /> 1,2-Dichloropropane NO 10 50 Comments
<br /> 1,3-Dichloropropane NO 10 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane NO 10 5 0 Dibromofluoromethane 97
<br />' 1,1-Dichloropropene NO 10 50 Toluene-d8 103
<br /> cis-1,3-Dichloropropene NO 10 50 4-Bromofluorobenzene 89
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> NO means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (c) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentaiione or isopropylacetone, (h)lighter than water immiscible sheen is present (i) liquid sample that contains greater than --5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene (m) acetic acid ethenyl ester, (n)
<br />' chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton, Lab Director
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