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I <br /> A-4 <br /> 4.0 SAMPLE CUSTODY <br /> This section describes standard operating procedures for sample custody and custody <br /> documentation. Sample custody procedures were followed through sample collection, transfer, <br /> analysis, and ultimate disposal. The purpose of these procedures is to assure that (1) the <br /> integrity of samples was maintained during their collection, transportation, and storage prior to <br /> analysis and (2) post-analysis sample material was properly disposed of. Sample custody is <br /> divided into field procedures and laboratory procedures, as described below. <br /> 4.1 Field Custody Procedures <br /> Sample quantities, types, and locations were determined before the actual fieldwork commenced. <br /> As few people as possible handled samples. The field sampler was personally responsible for <br /> the care and custody of the collected samples until they were properly transferred. <br /> 4.1.1 Field Documentation <br /> Each sample was labeled and sealed properly immediately after collection. Sample identification <br /> documents were carefully prepared so that identification and chain-of-custody records could be <br /> maintained and sample disposition could be controlled. Forms were filled out with waterproof <br /> ink. The following sample identification documents were utilized. <br /> • Sample labels <br /> • Field notebook <br /> • Chain-of-custody forms <br /> 4.1.2 Sample Labels <br /> Sample labels provide identification of samples. Preprinted sample labels were provided. <br /> Where necessary, the label was protected from water and solvents with clean label-protection <br /> tape. Each label contained the following information: <br /> • Name of collector <br /> • Date and time of collection <br /> • Place of collection <br /> • AMV project number <br /> • Sample number <br /> • Preservative (if any) <br /> 4.1.3 Field Noithook <br /> Information pertinent to a field survey, measurements, and/or sampling were recorded in a <br /> bound notebook. Entries in the notebook may have included the following: <br />