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' 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' J4E-mail mam@rnccampbell com <br />' Advanced GetiEnvironmental Client Project ID Larry Auto <br /> Date Sampled 08/12/99 <br /> 4005 North W11son Way Date Received 08/13/99 <br />' Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 08/16-08/17/99 <br /> Client P O Date Analyzed 08/16-08/17/99 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 17168 <br />' Client ID VW-SC <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ) ND<500 trans-l,3-Dichloropropene ND<500 <br />' Benzene 8900 Ethylene dibromide ND<500 <br /> Bromobenzene ND<500 Ethylbenzene 3600 <br /> Bromochloromethane ND<500 Hexachlorobutadiene ND<500 <br /> Bromodichloromethane ND<500 lodomethane ND<500 <br />' Bromofotm ND<500 1 sopropylbenzene ND<500 <br /> Bromomethane ND<500 p-lsopropyl toluene ND<500 <br /> n-Butyl benzene NIX500 Methyl butyl ketone` ND<500 <br /> sec-Butyl benzene NIX500 Methylene Chloride"' ND<500 <br /> tert-Butyl benzene NIX500 Methyl ethyl ketone NIX500 <br /> Carbon Disulfide ND<500 Methyl isobutyl ketones ND<500 <br /> Carbon Tetrachloride ND<500 Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<500 Naphthalene ND<500 <br /> Chloroethane ND<500 n-Propyl benzene 570 <br /> 2-Chloroethyl Vinyl Ether') ND<500 Styrene ND<500 <br /> Chloroform ND<500 1,1,1,2-Tetrachloroethane ND<500 <br /> Chloromethane ND<500 1,1,2,2-Tetrachloroethane ND<500 <br /> 2-Chlorotoluene ND<500 Tetrachloroethene ND<500 <br /> 4-Chlorotoluene ND<500 Toluene"' 15,000 <br /> Dibromochloromethane ND<500 1,2,3-Tnehlorobenzene ND<500 <br /> 1,2-Dibrorm-3-chloropropane ND<500 1,2,4-Tnchlorobenzene ND<500 <br /> Dibromomethane ND<500 1,1,1-Trichloroethane ND<500 <br /> 1,2-Dichlorobenzene ND<500 1,1,2-Tnchloroethane ND<500 <br /> 1,3-Dichlorobenzene ND<500 Trichloroethene ND<500 <br />' 1,4-Dichlorobenzene ND<500 Tnchlorofluoromethane ND<500 <br /> Dichlorodifluoromethane NIX500 1,2,3-Tnchloropropane ND<500 <br /> 1,1-Dichloroethane ND<500 1,2,4-Tnmethytbenzene 2900 <br /> 1,2-Dichloroethane ND<500 1,3,5-Tnmethylbenzene 960 <br /> IJ-Dichloroethene ND<500 Vinyl Acetate"I ND<500 <br /> cis-1,2-Dichloroethene ND<500 Vinyl Chlonde ° ND<500 <br /> trans-l,2-Dichloroethene ND<500 Xylenes,total 17,000 <br /> 1,2-Dichloropropane ND<500 Comments h <br />' 1,3-Dichloropropane ND<500 Surrogate Reco.eries(%) <br /> 2,2-Dichloropropane ND<500 I Dibromofluoromcthane 103 <br /> ]J-Dichloropropene NIX500 Toluene-d8 104 <br /> cis-1,3-Dichloropropene ND<500 4-Bromofluorobenzene 101 <br />' 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wrpe <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or rsopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certlficatlon No 1644 i Edward Hamilton,Lab Director <br />