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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> MCCANTBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> btm.//www mccam2belL= E-mail main@mccampbell corn <br /> Advanced GeoEnviromnental Client Project ID Larry Auto <br /> Date Sampled 08/12/99 <br /> 4005 North Wilson Way Date Received 08/13/99 <br /> Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 08116-08/17/99 <br /> Client P O Date Analyzed 08116-08117/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8250 <br /> Lab ID 17169 <br /> Client 1D MW-2 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<11 trans-l,3-Di chloropropene ND<ll <br /> Benzene 420 Ethylene dibromide NEXI 1 <br /> Bromobenzene ND<II Ethylbenzene 54 <br /> Bromochloromethane ND<l 1 Hexachlorobutadiene ND<1I <br /> Bromodichloromethane ND<11 lodomethane ND<l 1 <br /> Bromoform ND<11 ]sopropylbenzene ND<I1 <br /> Bromomethane ND<11 p-Isopropyl toluene ND<l 1 <br /> n-Butyl benzene ND<1 I Methyl butyl ketone ND<11 <br /> sec-Butyl benzene ND<l 1 Methylene Chloride"' ND<l 1 <br /> ten-Bury]benzene NEX)I Methyl ethyl ketone M ND<1I <br /> Carbon Disulfide ND<11 Methyl isobutyl ketone ND<l I <br /> Carbon Tetrachloride ND<l l Methyl tert-Butyl Ether(MTBE) --- <br /> Chlo obenzene ND<1I Naphthalene ND<l l <br /> Chloroethane ND<l I n-Propyl benzene ND<1 i <br /> 2-Chloroethyl Vinyl Ether` ND<ll Styrene ND<li <br /> Chloroform ND<11 1,1,1,2-Tetrachloroethane N D<1 i <br /> Chloromethane ND<11 1,1,2,2-Tetrachloroethane ND<l i <br /> 2-Chlorotoluene ND<l 1 Tetrachloroethane ND<ll <br /> 4-C hlorotoluene ND<l 1 Toluene"1 210 <br /> Dibromochloromethane NIX I 1 42,34n chlorobenzene N D<11 <br /> 1,2-Dibromo-3-chloropropane ND<I1 1,2,4-Tnchlorobenzene ND<ll <br /> Dibromomethane ND<11 1,1,1-Trichloroethane ND<l 1 <br /> 1,2-Dichlorobenzene N EX 11 1,1,2-Tnchloroethane ND<l 1 <br /> 1,3-Dichlorobenzene ND<11 Tnchloroethene ND<lI <br /> 1,4-Dichlorobenzene ND<11 Tnchlorofluoromethane ND<lI <br /> Dichlorodifluoromethane ND<11 1,2,3-Tnchloropropane ND<l 1 <br /> 1,1-Dichloroethane NEX 11 1,2,4-Tnmethylbcnzene 27 <br /> 1,2-Dichloroethane ND<l 1 1,3,5-Trimethylbenzene ND<11 <br /> l,]-Dichloroethene ND<l 1 Vinyl Acetate " ND<11 <br /> cis-1,2-Dichloroethene ND<l 1 Vinyl Chloride ND<I1 <br /> trans-1,2-Dichloroethene ND<11 Xylenes,total 180 <br /> 1,2-Dichloropropane ND<11 Comments <br />' 1,3-Dichloropropane ND<11 Surrogate Reco-teries(%) <br /> 2,2-Dichloropropane ND<l 1 Dibromofluoromethane 105 <br /> 1,I-Dichloropropene ND<l 1 Toluene-d8 105 <br /> cis-1,3-D chloropropene NEX I I 4-Bromofluorobenzenc 102 <br />' 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/"pe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />