Laserfiche WebLink
SOP TO-14A/15 <br /> Rev 4 <br /> December 2007 <br /> A Chain of Custody Record serves to note the disposition of the samples, from the time of collection to <br /> laboratory receipt. This form should be filled out at the time of collection and signed by all persons <br /> collecting, relinquishing and receiving samples. All samples must be documented on an appropriate Chain <br /> ' of Custody form. <br /> 15.2 Sample Run Lois <br /> ' H&P maintains a Sample Run Log for all samples analyzed. These logs are kept within a logbook, one of <br /> which is located in each van. A new log is prepared for each work day. The following information is <br /> ' included on the run logs: <br /> Date of operation <br /> ' H&Pjob number <br /> Operator name <br /> Instrument No. <br /> ' Analysis type <br /> Extraction method <br /> Duplicate information <br /> ' Sample data(sample amount,dilution factor, etc.) <br /> Calibration Standard identification <br /> Sample Analysis data <br /> ' Also located in each van are instrument and excursion logs. The instrument log is used to document <br /> problems and subsequent corrective action for the instrumentation (excessive column bleed, baseline <br /> ' irregularities, interference, etc.). The excursion log documents where and when the particular job takes <br /> place, the type of analysis, and operating conditions (weather, temperature, etc.). The excursion log should <br /> be filled out for each new job. <br /> ' 15.3 Reporting <br /> ' 15.3.1 The Data Package <br /> The analyst will prepare a data package for Reporting and Review. For EPA Method TO-14A/15 the <br /> t package will be produced on a daily basis corresponding to the 24-hour window of operations. The package <br /> will consist of the following in the order listed or as near as possible to that order: <br /> a) The Original COCs for the samples analyzed during that day <br /> ' b) The daily run logs <br /> C) The BFB tuning report <br /> d) Edited Quantitation reports from the daily initial Calibration (ICAL) or the passing <br /> ' Continuing Calibration Verification (CCV) <br /> e) The Response factor summary (if ICAL) or the Evaluation of CCV (if daily CCV) <br /> f) Edited quantitation report from the Initial Calibration verification (ICV) (If ICAL) <br /> ' g) ICV summary, if done showing all compounds<30%D <br /> h) Edited quantitation report from the LCS (if applicable) <br /> i) LCS Summary showing percent recovery and control limits(if applicable) <br /> ' Page 16 of 24 <br />