Laserfiche WebLink
• w <br /> [-� l McCamobell Analvfical, Inc. I334\ci0ot Pn.s,Ra,d.P:n,hare.rA 94565-1"01 <br /> ll, %k 6 ,,,mecnmpl d]trent E-mail,main/a.meoi npbelL coin <br /> "\1'hcntlunl:n Cnunte" Telehmre x77-252-9262 Fax.9332.2.9269 <br /> • QC SUMMARY REPORT FOR SW8270C <br /> W.O.Sample Matrix: Soil QC Matrix: Soil WorkOrder 0710131 <br /> EPA Method SW8270C Extraction SW3550C BatchID: 31040 Spiked Sample ID: 0710071-014A <br /> Analyte Sample Spiked MS MSC MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg % Rec. %Rea %RPD % Rec. %Rea %RPD MS/MSD RPD LCSILCSD RPD <br /> Acenaphthene ND 2 75,3 76.4 1.41 82.3 82.2 0.0730 30- 130 30 30- 130 30 <br /> 4-Chloro-3-methvlhenol ND 4 72.3 723 0 75.9 73.3 3.43 30- 130 30 30- 130 30 <br /> 2-Chlorophenol ND 4 81.3 80.7 0.772 75.6 74.7 1.21 30- 130 30 30- 130 30 <br /> 1,4-Dichlorobenzene ND 2 77.1 77Si 0.737 84.6 84 0.629 30- 130 30 30- 130 30 <br /> 2.4-Dinitiotoluene ND 2 72.3 73.3 1.32 77.2 77 0.285 30- 130 30 30- 130 30 <br /> 4-Nitro phenol ND 4 76.3 78.9 3.42 84 84.6 0.765 30- 130 30 30- 130 30 <br /> N-Nitrosodi-n- ro olamine ND 95.8 92.3 3.69 73 74.4 1.79 30- 130 30 30- 130 30 <br /> Pentachlorophenol NO 4 60.9 60.6 0.387 69.1 68.8 0.3_'6 30- 130 30 30- 130 30 <br /> Phenol ND 4 69.4 68.1 1.93 73.7 71.1 3.70 30- 130 30 30- 130 30 <br /> Pvrene ND 2 78.9 81.1 2.77 88.7 89.3 0.686 30- 130 30 30- 130 30 <br /> 1,2,4-Tnehlonncen,cns' NO 2 85.8 89 3.60 91.6 93.1 1.64 30- 130 30 30- 130 30 <br /> %SSI: 84 200 86 87 0.746 82 80 3.31 30- 130 30 30. 130 30 <br /> %SS2: 70 200 74 78 4.54 85 74 14.4 310. 130 30 30. 130 30 <br /> %SS3: 93 200 94 97 3.75 108 109 0.764 10- 130 30 30- 130 30 <br /> 6/*SS4: 79 200 78 79 0.G33 92 92 0 30- 130 30 30- 130 30 <br /> %SS5: 74 200 69 71 2.48 69 53 26.0 30- 130 30 30- 130 30 <br /> %SS6: 1 80 200 79 81 2.08 97 97 0 30- 130 30 30- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were NO less than the method Rl-with the following exceptions: <br /> NONE <br /> BATCH 31040 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 0710131.00IA 10/03/07 8:36 AM 10/03/07 10/05/07 12:14 AM 0710131-002A 10/03/07 8:47 AM 10/03/07 10/05/07 1:30 AM <br /> (1710131-003A 10/03/07 9:47 AM 10/03/07 IOi04107 10:55 PM 0710131-004A 10/03/07 10:11 AM 10/03/07 30/05./07 12:13 AM <br /> 07 1013 1-005A 10/03/07 10:19 AM 10/03/07 10/05/07 1:31 AM 0710131-006A 10/03/07 10:22 AM 10/03/07 10/05/07 2:48 AM <br /> 0710131-007A 10/03/07 10:42 AM 10/03/07 10/05/07 4:05 AM <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons.a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> IA=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyle concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS EI-AP Certification No IW '-W- QA/QC Officer <br />