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0 0 <br /> McCamnbell AnaNtical, Inc. 15341 itov Pas Road Pinshura CA94565-1701 <br /> (( 11'rk wt%,mccampbellmm E-mail:mninfpmmccamplaell,com <br /> `lIIU%� <br /> "Mhcauauili,('.um" ldmhone_877-22-9262 lax:925-252-9269 <br /> • QC SUMMARY REPORT FOR SVV8270C <br /> W.O.Sample Matrix: Soil OC Matrix: Soil WorkOrder 0710131 <br /> EPA Method SW8270C Extraction SW3550C BatchlD: 31084 Spiked Sample ID: 0710131-008A <br /> Analyte Sample Spiked MIS MSC MS-MSD LOS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg %Rec. %Rec. %RPD %Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> Acene hthene ND 2 77.6 78.2 0.847 93.3 9.7.5 0.204 30- 130 30 30- 130 30 <br /> 4-Chloro-3-methvlphenol NO 4 81.4 83.4 2.43 90.7 91.7 1.05 30- 130 30 30- 130 30 <br /> 2-Chlorophenol ND 4 86.6 57.5 1.01 89 88.6 0.490 110- 130 30 30- 130 30 <br /> 1.4-Dichlorobenzene ND 2 1 79.8 80.6 0.935 88.6 88.4 0.158 30- 130 30 .10- 130 30 <br /> '_.4•Dinilrotoluene ND 79.2 79.5 (1.290 89.9 90.5 0.599 30- 130 30 30- 130 10 <br /> 4-Nitrophenol ND 4 70.5 67.9 3.75 74.1 70.6 4.87 30- 130 30 30- 130 30 <br /> N-Nitrosodi-n- ro olamine NU I110 110 0 17A 54.4 5.44 30. 130 30 30- 130 30 <br /> Pentachlorophenol ND 4 62.8 65.2 3.68 59 61.4 4.04 30- 130 30 30- 130 30 <br /> Phenol ND 4 80.5 79.7 1.01 88.5 85.5 3.47 30- 130 30 30- 130 30 <br /> Pvrcne ND 2 80.4 82.7 2.77 91.5 88.3 3.62 30- 130 30 30- 130 30 <br /> 1.2,4-Trichlorobenzene ND 1 87.1 8 8.31 1.39 93.5 94.8 1.41 30- 130 30 30- 130 30 <br /> %SSI: 92 200 92 93 1.77 96 96 11 i0- 130 30 30. 130 30 <br /> %SS2: 91 200 83 78 6.35 97 95 r 32 .110- 1.110 30 30- 130 30 <br /> %SS3: 99 200 100 102 1.21 103 103 0 l0- 130 30 30- 130 30 <br /> %SS4: 79 200 81 81 0 95 95 0 310- 1.110 30 30- 130 30 <br /> %SS5: 88 200 84 89 5.75 90 92 2.47 30- 130 30 30- 130 30 <br /> %SS6: 79 200 79 80 1.71 1 94 91 3.14 30- 130 30 30- 130 1 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 31084 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 071013 1.008A 10 03/07 10:25 AM 10/03/07 10/04/07 8:27 PM <br /> MS=Matrix Spike:MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate:RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked),RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of anahle relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content <br /> DHS ELAP Certification No 1044 "W-- QA'Q(()flicei <br />