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C. Equignent Decontamination <br /> * EPA Region 9 recommended generic procedure prior to initial sampling. <br /> 1) Wash w/ non—phosphate detergent. <br /> 2) Tap water rinse <br /> 3) 0.1N nitric acid rinse <br /> 4) Deionized/distilled water rinse <br /> 5) Pesticide grade solvent rinse <br /> 6) Deionized/distilled water rinse (2x) <br /> 7) organic free water rinse (HPLC grade) <br /> * Decontamination in the field may not require a nitric acid rinse. <br /> * You may want to use a different procedure. Give the rationale. <br /> * Acetone is not recommended for the solvent rinse since it is one of the <br /> compounds on the TCL. If acetone or any other TCL canpound is used as part <br /> of the decontamination process then the Sample Plan should discuss this <br /> and note that the solvent in question is not a ccmpound of interest. <br /> * Whenever possible, obtain sets of each sampling tool being used in the field <br /> so that decontamination can done in batches, after all the equipment has <br /> been used. This will minimize the number of blanks needed. <br /> D. Sample Containers <br /> * Identify the container types that will be used for each of the analytical <br /> parameters and the source of sample containers. Identify the parameters <br /> which will be combined in sample containers. Make sure that the preservation <br /> rewirements are canpatible and the sample volume will be sufficient. <br /> * Appendix C identifies the containers and volumes which are required for <br /> the CLP RAS analyses. Containers provided by the CLP should not be rinsed <br /> before s anpling. <br /> * For SAS analyses, collect at least twice the minimum volume required by the <br /> analytical method (see Appendix D) . In sane cases, a special type <br /> or zed <br /> container is required for SAS analyses. <br /> E. Sample Preservation <br /> * Appendix D identifies sane preservation methods. Detail the methods to be <br /> used in your Sample Plan. Identify when they will be implemented. <br /> * The preservatives used must be indicated on the sample container and on the <br /> paper work. <br /> * Region 9 is now requiring, for CLP samples, acidification of low concentration <br /> croundwater and other drinking water samples for analysis by EPA method 601. <br />