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ii <br /> 05 December 2008 <br /> AGE-NC Project No. 04-1153 <br /> Page 2 of 5 <br /> of the second or other selected sleeve were covered with Teflon sheets,capped,and sealed with tape. <br /> Samples were labeled, stored on ice, and transported under chain-of-custody to Cal Tech <br /> Environmental Laboratories (CTEL) a State of California Department of Public Health (CDPH)- <br /> certified analytical laboratory. Selected samples were analyzed for: <br /> • Total petroleum hydrocarbons as gasoline (TPH-g), as diesel (TPH-d), and as oil (TPH-o) <br /> in accordance with EPA Method 8015 Modified; and <br /> • Benzene, toluene, ethylbenzene and total xylenes (BTEX), and fuel additives methyl-tert- <br /> butyi ether(MTBE), tertiary butyl alcohol (TBA), di-isopropyl ether (DIPE), ethyl tertiary <br /> butyl ether (ETBE), tertiary amyl methyl ether (TAME), 1,2-dibromoethane (EDB), and <br /> 1,2-dichloroethane (1,2-DCA) in accordance with EPA Method 8260B. <br /> All sampling equipment was washed in an Alconox solution and rinsed twice with water prior to <br /> each sampling run.All rinseate generated by drilling-related activities was containerized in properly <br /> labeled department of transportation (DOT)-approved 55-gallon drams, was taken off-site, and <br /> stored until it could be properly disposed. All soil borings were backfilled over their entire depth <br /> with either a Portland cement grout mix or a Portland cement slurry. <br /> 2.3. SOIL LOGGING <br /> After sample preservation, soil was extruded from!the remaining sleeves. Soils were visually <br /> classified by an AGE geologist in accordance with the Unified Soil Classification system. <br /> Additionally, soils were screened for the presence of.volatile organic compounds using an organic <br /> vapor analyzer(OVA) equipped with a photo-ionization detector(PID)calibrated to an appropriate <br /> isobutylene standard. Boring logs exhibiting soil profiles are depicted in Appendix C. <br /> 2.4. GRAB GROUND WATER COLLECTION AND ANALYSIS <br /> After completing the boring,the ground water table was measured and observed to be approximately <br /> 45 feet bsg. One `grab' ground water sample was collected from boring B2. Ground water was <br /> extracted by hand bailing the boring with disposable '/4-inch tubing and sampling check valve. The <br /> ground water sample was transferred into three laboratory-supplied,40-m1 volatile organic analysis <br /> (VOA) vials, and one laboratory-supplied 1-liter amber bottle. After collection, the sample was <br /> properly labeled, placed in a chilled container, and transported under chain-of-custody to CTEL. <br /> Samples were analyzed for the constituents listed in Section 2.2. <br /> Advanced GeoEnvironmental,Inc. <br />