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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' 4 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell com E-mail main@mccampbell corn <br />' Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/30/01 <br /> 837 Shaw Road Date Received 12/04/01 <br />' Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/07-12/11/01 <br /> [Clientp O Date Analyzed 12/07-12/11/01 <br /> I Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 84747 <br /> Client ID P18(20-24)/113001 <br /> Matrix W <br /> Reporting Limit Reporting Limit <br />' Compound Concentration* W S Compound Concentration* W s <br /> Acetone tel NDc10 50 25 trans-l,3-Dtehloropropene ND 1 0 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 1 0 5 0 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 1 0 5 0 <br /> Bromochloromethane ND 10 5 0 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 10 50 lodomethane ND 10 50 <br /> Bromoform ND 1 0 5 0 Isopropylbenzene ND 1 0 50 <br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 1 0 50 <br /> Ti-Butyl benzene ND i 0 5 0 Methyl butyl ketone ND 1 0 5 0 <br /> see-Butyl benzene ND 10 5 0 Methylene Chlondct` ND<2 0 1 0 5 0 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 2 0 t0 <br /> • Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone`e ND 1 0 50 <br /> Carbon Tetrachloride ND 10 50 Methyl tert-Butyl Ether(MTBE) 10 5 0 <br /> Chlorobenzene ND 10 50 Naphthalene ND 50 25 <br /> Chloroethane ND 10 50 n-Propyl benzene ND l 0 50 <br /> 2-Chloroethyl Vinyl Ether"' ND 10 5 0 Styrene` ND 1 0 50 <br /> Chloroform ND 10 5 0 1,1,1,2-Tetrachloroethane ND 1 0 50 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 1 0 5 0 <br /> 2-Chlorotoluene VD 1 0 5 0 Tetrachloroethene ND 1 0 5 0 <br />' 4-Chlorotolume ND 1 0 50 Toluene ND 10 50 <br /> Dibromochloromethane ND 10 5 0 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Trichlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 50 1,1,1-Tnchloroethane ND 10 50 <br /> I 1,2-1)ichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND 10 50 <br /> 1 3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 1 0 50 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Tnchlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Trichioropropane ND 1 0 50 <br /> 1,1-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1 2-Dichloroethane ND 1 0 50 1,3,5-Ttimethylbenzene ND 10 50 <br /> l,1-Dchloroethene ND 10 50 Vinyl Acetate lm - ND 5 0 25 <br /> css-1,2-Dichloroethene ND 1 0 50 Vinyl Chlonde °' ND 10 5 0 <br /> trans-l,2-Dichloroethene ND 1 0 50 Xylenes,total ND 1 0 5 0 <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 13-Dichloropropane ND 1 0 5 0 Surrogate Recoveries{'%) <br /> 2,2-Dichloropropane ND 1 0 50 Dsbromofluoromethane 102 <br /> I 1,1-Dichloropropene ND to 50 Toluene-d8 98 <br /> cis-1,3-Dwhloropropene 11ND 10 50 4-Bromofluorobenzene 96 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting lirml,N/A means analyte not apphcable to this analysis <br /> . (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pmtanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />