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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAIVIPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htt-p wrn lE-mail main@mccampbell coin <br /> //ww o bel com <br /> Advanced GeoEnvironrnental Client Project lD Three B's Date Sampled 11/30/01 <br /> 837 Shaw Road Date Received 12/04/01 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/07-12/11/01 <br /> Client P O Date Analyzed 12/07-12/11/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 84747 <br /> Client ID P18(20-24)/113001 <br /> Matrix W <br /> Compound Concentration* ReportsngLun:t Compound Concentration* ReportingLmui <br /> W S W 5 <br /> Acetone(b) NDS10 50 25 trans-1,3-Dtchloropropene ND 10 50 <br /> Benzene ND 10 0 Ethylene dibromide ND -10 5 0 <br /> I Bromobenzene ND 10 50 Ethylbenzene ND 10 5 0 <br /> Bromochloromethane ND 10 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 5 0 lodomethane ND 1 0 50 <br /> Bromoform ND 10 50 Isopropylbenzene ND 10 50 <br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 10 5 0 <br /> n-Butyl benzene ND 10 5 0 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND to 5 0 Methylene Chlondet` ND<2 0 1 0 50 <br /> tent-Butyl benzene ND l 0 5 0 Methyl ethyl ketone ND 2 0 10 <br /> • Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone v ND 10 50 <br /> Carbon Tetrachlonde ND 10 50 Methyl tert-Butyl Ether(MTBE) 1 0 5 0 <br /> Chlombenzene ND 10 50 Naphthalene ND 50 25 <br /> Chioroethane ND 10 50 n-Propyl benzene ND 10 5 0 <br /> 2-Chloroethyl Vinyl Eth ` ND 10 5 0 Styrene ND 10 5 0 <br /> Chloroform ND 10 5 0 1,1,1,2-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 10 5 0 1,1,2,2-Tetrachloroethane ND 10 5 0 <br /> 2-Chlorotoluene ND 10 5 0 Tetrachloroethane ND 1 0 5 0 <br /> 4-Chlorotaluene ND 10 5 0 Toluene SID 10 5 0 <br /> Dibromochloromethane ND 10 5 0 1,2,3-Tnchloroberizene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropano ND 2 0 10 1,2,4-rrichlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 5 0 1,1,1-Tnchloroethane ND 1 0 5 0 <br /> 1,2-Dichlorobenzene ND 10 5 0 1,I,2-Tnchloroethane ND 1 0 )o <br /> 1,3-Dichiorobenzene ND 10 5 0 Trichloroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND 10 5 0 Tnchloratluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Tnehloropropane ND 10 5 0 <br /> I l,l-Dichloroethane ND 10 5 0 12,4-Tnmethylbenzene ND 10 5 0 <br /> 1,2-Dichioroethane ND 10 5 0 1,3,5-Tnmethylbenzene ND 10 5 0 <br /> 1 1-Dichloroethene ND 10 50 Vinyl Acetate m - ND 5 0 25 <br /> cis-1,2-Dichioroethene ND 10 5 0 Vinyl Chloride to ND 10 5 0 <br /> trans-l,2-Dichloroethme ND 10 5 0 Xyienes,total ° ND to 5 0 <br /> 1,2-Dichloropropane ND 1 0 5 0 Comments <br /> 1,3-Dtchloropropane ND 1 0 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane 102 <br /> 1,1-Dtchloropropene ND 10 50 Toluene-dg 98 <br /> cis-1,3-Dtchloropropene ND 1 0 50 1 4-Bromotluorobenzene 96 <br /> water and vapor samples are reported to ug/L,soil and sludge samples to ug/kg,wipes to ug/wipe and all TCLP 1 SPLP extracts m ug/L <br /> ND means not detected above the reporting lirrul,N/A means analyte not applicable to this analysts <br /> • (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Directot <br />