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I <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' F14 McCAMTBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htt�_//www mccampbell cora E-mail matn@mccampbell com <br />' Advanced GeoEiivironinental Client Project ID Three B's Date Sampled 11/30/01 <br />' 837 Shaw Road Date Received 12/04/01 <br /> Stockton, CA 95215 Client Contact Tire Cuellar Date Extracted 12/07-12/11/01 <br />' Client P O Date Analyzed 12/07-12/11/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 84748 <br /> Client ID P18(42-46)/113001 <br /> Matrix W <br /> I Compound Concentration* Reporting Limt Compound Concentration* Rcp mng t,rmt <br /> Acetone tet ND<10 50 25 trans-l,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 10 5 0 Ethylene dibromide ND 10 5 0 <br />' Bromobenzene ND 10 50 Ethylbenzene ND to 5 0 <br /> Bromochlommethane ND 10 5 0 Hecachlorobutadiene 'SID 50 25 <br /> Bromodichloromethane ND 10 5 0 Iodomethane ND 1 0 3 0 <br /> Bromoform ND l 0 5 0 lsopropylbenzene ND 10 50 <br /> I Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketoneND 10 5 0 <br /> Sec-Butyl benzene ND 10 5 0 Methylene Chlonde e ND<2 0 1 0 5o <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 2 0 10 <br /> • Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone 191 ND 1 0 50 <br /> Carbon Tetrachlonde ND 10 5 0 Methyl tert-Butyl Ether(MTBE) 10 5 0 <br /> Chlorobenzene ND 10 5 0 Naphthalene ND 5 0 25 <br /> Chloroethane ND 10 50 n-Propyl benzene ND 1 D 50 <br /> 2 Chloroethyl Vinyl Ether') ND 10 50 Styrene') ND 10 50 <br /> Chloroform ND 10 5 0 1 1 1,2-Tetrachloroetliane ND 10 50 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chlorotoluene ND 10 50 Tcu=hloroethene ND 10 50 <br /> 4-Chlorotoluene ND 10 5 0 Toluene ND 1 0 5 0 <br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Trichlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 50 1 1 1-Tnehloroethane ND 1 0 5 0 <br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Trichloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 10 50 <br /> 1 4-Dichlorobenzene ND 10 5 0 4 Trtchlorolluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Tnehloropropane ND 10 5 0 <br /> 1,1-Dichloroethane ND 10 1 50 t,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 10 5 0 1,3,5-Tnmethylbenzene ND 1 0 5 0 <br /> IJ-Dichloroethcne ND 10 50 Vinyl Acetate m ND 5 0 25 <br /> cis-1 2-Dichloroethene ND 10 50 Vinyl Chloride " ND 10 50 <br /> trans-1,2-Dichloroethene ND 10 5 0 Xylencs,total ND 1 0 S U <br /> 1,2-Dichloropropane ND 1 0 5 0 Comments <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 50 Dibromotluoromethane 103 <br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 98 <br /> cis-1,3-Dtchloropropene ND 10 50 1 4-13romofluorobenzene 95 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in us/l, <br /> I ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chlomethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i) liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />