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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> . http//www mccaMbelI corn E-mail main@mccampbell com <br />' Advanced GeoEnvtronmental Client Project ID Three B's Date Sampled 11/30/01 <br /> 837 Shaw Road Date Received 12/04/01 <br />' Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/07-12/11/01 <br />' Client P O Date Analyzed 12/07-12/11/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 84749 <br /> Client ID P18(72-76)/113001 <br /> Matrix W <br /> Reporting Limit Report=ng Limit <br />' Compound Concentration* W S Compound Concentration* W 5 <br /> Acetone 1bi ND<0 50 25 trans-l,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 1 0 50 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 1 0 50 <br /> Bromochloromethane ND 10 50 Herachlorobutadiene ND 50 25 <br /> Bromodichioromethane ND 10 50 Iodomethane ND 1 0 50 <br /> Bromoform ND l 0 50 Isopropylbenzene ND 1 0 5 0 <br /> Bromomethane ND 1 0 50 p4sopropyl toluene ND l 0 50 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND l 0 5 0 <br /> sec-Butyi benzene ND 10 50 Methylene Chlonde e ND<2 0 1 0 5 0 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone` ND 20 10 <br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone is ND 1 0 5 0 <br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) 1 0 5 0 <br /> Chlorobenaene ND 10 50 Naphthalene ND 50 25 <br /> Chloroethane ND 10 56 n-Propyl benzene ND 1 0 5 0 <br /> 2-Chloroethyl Vinyl Ether' ND 10 50 Styrene ND 1 0 50 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane VD 1 0 50 <br /> Chloromethane ND 10 50 1 1 2,2-Tetrachloroethane ND 1 0 50 <br /> 2-Chlorotoluene ND 10 50 Tetrachloroethene ND 1 0 50 <br /> 4-Chlorotoluene ND 1 0 50 Toluene ND 1 0 5 0 <br /> Dibromochloromethane ND 1 0 50 1,213-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 2� <br /> Dibromomethane ND 10 50 1,1 1-lnchloroethane ND 1 0 5 0 <br /> I l 2-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND 1 0 5 0 <br /> 1,3-Dichlorobenzene ND 10 50 Trichloroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND 1 0 5 0 <br /> Dichlorodtfluoroinethane ND 1 0 50 1,2,3-Tnchloropropane ND 1 0 50 <br /> IJ-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzene ND 1 0 50 <br /> IJ-Dichloroethene ND 10 56 Vinyl Acetate ND 50 25 <br /> cis-1,2-Dichloroethene ND 10 50 Vinyl Chloride ° ND 1 0 50 <br /> I trans-l,2-Dichloroethene ND 10 50 Xylenes,total ° ND ] 0 5 0 <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 50 Dibromotluoromethane 102 <br /> 1 I-Dichloropropene ND 10 50 Toluene-d8 98 <br /> cis-1,3-Dichloropropene ND 10 50 4-Bromofluorobenzene 94 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> IND means not detected above the reporting limit,NLA means analyte not applicable to this analysis <br /> . (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (t) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (b) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol 0A <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloraethene (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />