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1102nd Avenue South,#D7,Pacheco, CA 94553-5560 <br />' F4 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 http//www mceamobell coin E-mail main@mecampbell corn <br />' Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/26-11/27/01 <br /> 837 Shaw Road Date Received 11/30/01 <br />' Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/03-12/06/01 <br />' Client P O Date Analyzed 12/03-12/06/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 84513 <br /> Client ID CPT13(76-80)/112601 <br /> Matrix W <br /> * Reporting Limit Reporting Limit <br /> W S <br />' Compound Concentration* Compound Concentrahan* <br /> W S <br /> Acetone e' ND<15 50 25 trans-1,3-Dichloropropene ND 10 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 1 0 5 0 <br /> Bromobenzene ND 1 0 5 0 Ethylbenzene ND l 0 5 0 <br /> Bromochloromethane ND 1 0 5 0 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 5 0 Iodomethane ND 1 0 50 <br /> Bromoform ND 1 0 50 Isopropytbenzene ND 1 0 50 <br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 1 0 5 0 <br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 1 0 5O <br /> sec-Butyl benzene ND 1 0 50 Methylene Chloride"' ND<2 0 1 0 5 0 <br /> tent-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone d' ND l 0 50 <br /> Carbon Tetrachloride ND 10 50 Methyl tert-Butyl Ether{MTBE) 10 -')o <br /> Chlorobenzene ND 10 50 Naphthalene ND 50 25 <br /> Chloroethane ND 1 0 55- n-Propyl benzene ND 1 0 5 0 <br /> 2-Chlorcethyl Vinyl Ether ivD 1 0 5o Styrene IV,, ND 1 0 5 0 <br /> Chloroform ND 1 0 5 0 1,1,1,2-Tetrachloroethane ND 1 D 5 0 <br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND I o 5 0 <br /> 2 Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 1 0 5 0 <br /> 4-CNorotoluene ND 1 0 50 Toluene ND 1 0 1 5 4 <br /> Dibromochioromethane ND 1 0 50 1,2,3-Trichlorobenzene ND 5 0 25 <br /> t 2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Trichloroethane ND 1 0 5 0 <br /> 1,2-Du,hlorobenzene ND 1 0 5 0 1,1,2-Tnchloroethane ND 1 0 5 0 <br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Trichlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Tnchloropropane ND 1 0 5 0 <br /> l,l-Dichloroethane ND 1 0 5 0 1,2,4-Trimethylbenzene ND 1 0 5 0 <br /> 1 2-Diclilorcerhane ND 1 0 50 1,3,5-Trimethylbenzene ND to 50 <br /> 1,1-01chloroethene ND 1 0 50 Vinyl Acetate " _ ND 50 25 <br /> cis-1,2-Dichioroethene ND two 50 Vinyl Chloride " ND 1 0 5 6 <br /> trans-l,2-Dichloroethene ND l 0 5 0 Xylenes,total ND 1 0 5 0 <br /> 1,2-Dtchloropropane ND I 0 50 Comments <br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%) <br /> 2,2-Dtchloropropane ND L10 <br /> 5 0 Dibromofluoromethane 115 <br /> [,I-Dtchloropropene ND 50 Toluene-d$ 94 <br /> cis-l,3-Dichloropropene ND 5 0 4-Bromof3uorobenzene 100 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts to ug/L <br /> I ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (1) liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene 1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> E t.hloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />