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10.3.1 .2 INDIVIDUAL TRUCK ALIQUOTS <br /> A minimum of four (4) of the samples from each truck will be analyzed as outlined below: <br /> • TTLC and STLC for Metals (lead, arsenic and copper) via EPA Method 6010B. <br /> • TCLP for lead via EPA Method 1311. <br /> • pH via EPA Method 9040, EPA Method 9045 (calcareous procedure not used) or <br /> other approved test method described in SW-846. (DTES will analyze more than <br /> four (4) samples if SW-846, Table 9-1, Equation 8, provides that a higher number <br /> of samples is appropriate.) <br /> In addition, One (1) of the four (4) samples will have California Title 22 metals (also called <br /> CAM 17) metals analysis. This is to confirm other metals, other than those outlined above, <br /> are below regulatory limits. The metals listed above are more likely to be present in the <br /> ash at higher concentrations than the rest of the CAM 17 metals. <br /> The remaining four (4) samples will be retained on site in the event additional laboratory <br /> analyses are necessary. <br /> 10.3.2 STATISTICAL ANALYSIS <br /> The individual truck aliquots results will be used to calculate an 80% confidence interval <br /> for each truck. For non-detect ("ND") values the Method Detection Limit ("MDL") will be <br /> used. <br /> Once the calculations have been completed for the all of the sampled trucks, DTES will <br /> use this information to make a Generator Knowledge determination if the ash can reliably <br /> be characterized as non-hazardous for the following quarter. <br /> At DTES' option, the additional samples collected from each truck may be analyzed and <br /> included in the 80% confidence interval calculation. <br /> Bottom ash, from the trucks sampled, will be considered Nonhazardous Ash as long as <br /> the values of the 80% confidence intervals for each constituent and parameter are below <br /> the applicable regulatory thresholds. <br /> If the bottom ash is considered hazardous DTES will dispose of and transport the Ash as <br /> Hazardous Waste. DTES will then conduct a fuel quality review as outlined in Section <br /> 7.1. Once the fuel quality review has been conducted, DTES will repeat the sampling <br /> process outlined in Section 10.0 over a period of two weeks instead of one week. If the <br /> upper value for the 80% confidence interval for each constituent and parameter are below <br /> the applicable regulatory thresholds, then the Ash can be managed as non-hazardous. If <br /> the confidence intervals exceed regulatory thresholds, the Ash will be managed as <br /> hazardous waste until the problem with the fuel is identified and remedied. At that point, <br /> the sampling process outlined in Section 10.0 will be repeated again for two weeks to <br /> calculate the 80% confidence interval. <br /> 27 <br />