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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-002-SA Date Extracted: 04-16-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-2 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 0.668
<br />Matrix: Solid Amount: 5.03 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4473 % Solids: 94.12
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.209 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.390 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.353 -0.0793
<br />1,2,3,6,7,8-HxCDD 1.12 - J 0.112 0.0940 Total TCDD 0.542 -J
<br />1,2,3,7,8,9-HxCDD 0.700 - J 0.0700 0.0823 Total PeCDD ND 0.390
<br />1,2,3,4,6,7,8-HpCDD 16.1 -0.161 0.0842 Total HxCDD 6.96 -
<br />OCDD 126 -0.0378 0.172 Total HpCDD 30.6 -
<br />2,3,7,8-TCDF 0.628 - J 0.0628 0.0269
<br />1,2,3,7,8-PeCDF ND 0.182 -0.0449
<br />2,3,4,7,8-PeCDF 0.464 - J 0.139 0.0468
<br />1,2,3,4,7,8-HxCDF 0.443 - J 0.0443 0.0437
<br />1,2,3,6,7,8-HxCDF ND 0.193 - 0.0417
<br />2,3,4,6,7,8-HxCDF ND 0.222 - 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.238 -0.0657 Total TCDF 2.57 -
<br />1,2,3,4,6,7,8-HpCDF 3.80 - J 0.0380 0.0747 Total PeCDF 3.62 -J
<br />1,2,3,4,7,8,9-HpCDF ND 0.255 -0.0883 Total HxCDF 4.88 -J
<br />OCDF 9.14 - J 0.00274 0.170 Total HpCDF 9.45 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 92.1 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 95.3 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 98.1 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 96.1 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 93.3 23.0 - 140
<br />13C-OCDD 83.7 17.0 - 157
<br />13C-2,3,7,8-TCDF 94.5 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 88.7 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 89.5 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 91.8 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 89.3 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 89.3 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 88.4 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 90.7 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 91.9 26.0 - 138
<br />13C-OCDF 82.0 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 82.6 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/18/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />4/18/2018
<br />000008 of 000033
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