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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-003-SA Date Extracted: 04-16-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-3 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 1.10
<br />Matrix: Solid Amount: 5.02 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4473 % Solids: 94.41
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.194 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.281 -0.0570
<br />1,2,3,4,7,8-HxCDD 0.702 - J 0.0702 0.0793
<br />1,2,3,6,7,8-HxCDD 1.47 - J 0.147 0.0940 Total TCDD 0.443 -J
<br />1,2,3,7,8,9-HxCDD 1.04 - J 0.104 0.0823 Total PeCDD 0.610 -J
<br />1,2,3,4,6,7,8-HpCDD 24.3 -0.243 0.0842 Total HxCDD 9.86 -
<br />OCDD 194 -0.0582 0.172 Total HpCDD 45.0 -
<br />2,3,7,8-TCDF 1.01 -0.101 0.0269
<br />1,2,3,7,8-PeCDF ND 0.241 -0.0449
<br />2,3,4,7,8-PeCDF 0.515 - J 0.155 0.0468
<br />1,2,3,4,7,8-HxCDF 0.630 - J 0.0630 0.0437
<br />1,2,3,6,7,8-HxCDF 0.422 - J 0.0422 0.0417
<br />2,3,4,6,7,8-HxCDF 0.601 - J 0.0601 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.248 -0.0657 Total TCDF 3.15 -
<br />1,2,3,4,6,7,8-HpCDF 5.11 -0.0511 0.0747 Total PeCDF 4.92 -J
<br />1,2,3,4,7,8,9-HpCDF ND 0.262 -0.0883 Total HxCDF 7.74 -
<br />OCDF 14.0 -0.00420 0.170 Total HpCDF 13.6 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 84.7 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 89.7 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 93.0 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 90.3 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 83.4 23.0 - 140
<br />13C-OCDD 66.9 17.0 - 157
<br />13C-2,3,7,8-TCDF 89.1 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 87.3 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 86.4 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 86.8 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 83.2 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 78.8 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 80.5 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 83.0 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 81.9 26.0 - 138
<br />13C-OCDF 71.1 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 81.6 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/18/2018 4/18/2018
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