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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-004-SA Date Extracted: 04-16-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-4 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 0.510
<br />Matrix: Solid Amount: 5.02 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4473 % Solids: 95.60
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.212 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.388 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.340 -0.0793
<br />1,2,3,6,7,8-HxCDD 0.999 - J 0.0999 0.0940 Total TCDD ND 0.212
<br />1,2,3,7,8,9-HxCDD 0.825 - J 0.0825 0.0823 Total PeCDD ND 0.388
<br />1,2,3,4,6,7,8-HpCDD 18.1 -0.181 0.0842 Total HxCDD 7.26 -
<br />OCDD 166 -0.0498 0.172 Total HpCDD 33.2 -
<br />2,3,7,8-TCDF 0.653 - J 0.0653 0.0269
<br />1,2,3,7,8-PeCDF ND 0.216 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.237 -0.0468
<br />1,2,3,4,7,8-HxCDF ND 0.439 -0.0437
<br />1,2,3,6,7,8-HxCDF ND 0.443 - 0.0417
<br />2,3,4,6,7,8-HxCDF ND 0.469 - 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.517 -0.0657 Total TCDF 3.18 -
<br />1,2,3,4,6,7,8-HpCDF 2.92 - J 0.0292 0.0747 Total PeCDF 2.42 -J
<br />1,2,3,4,7,8,9-HpCDF ND 0.236 -0.0883 Total HxCDF 3.80 -J
<br />OCDF 6.59 - J 0.00198 0.170 Total HpCDF 7.14 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 84.2 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 92.2 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 90.2 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 87.9 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 84.0 23.0 - 140
<br />13C-OCDD 70.6 17.0 - 157
<br />13C-2,3,7,8-TCDF 88.8 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 85.6 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 87.6 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 83.6 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 81.6 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 80.5 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 80.5 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 82.0 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 83.4 26.0 - 138
<br />13C-OCDF 73.0 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 80.7 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/18/2018 4/18/2018
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