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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-005-SA Date Extracted: 04-16-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-5 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 4.88
<br />Matrix: Solid Amount: 5.05 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4473 % Solids: 96.53
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.245 - 0.0273
<br />1,2,3,7,8-PeCDD 0.682 - J 0.682 0.0570
<br />1,2,3,4,7,8-HxCDD 1.44 - J 0.144 0.0793
<br />1,2,3,6,7,8-HxCDD 5.76 -0.576 0.0940 Total TCDD 0.702 -J
<br />1,2,3,7,8,9-HxCDD 2.92 - J 0.292 0.0823 Total PeCDD 7.92 -M
<br />1,2,3,4,6,7,8-HpCDD 152 -1.52 0.0842 Total HxCDD 43.4 -
<br />OCDD 1540 -0.462 0.172 Total HpCDD 280 -
<br />2,3,7,8-TCDF 2.49 - F 0.249 0.0269
<br />1,2,3,7,8-PeCDF 0.683 - J 0.0205 0.0449
<br />2,3,4,7,8-PeCDF 1.25 - J 0.375 0.0468
<br />1,2,3,4,7,8-HxCDF 1.31 - J 0.131 0.0437
<br />1,2,3,6,7,8-HxCDF 1.22 - J 0.122 0.0417
<br />2,3,4,6,7,8-HxCDF 1.38 - J 0.138 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.276 -0.0657 Total TCDF 15.5 -
<br />1,2,3,4,6,7,8-HpCDF 13.8 -0.138 0.0747 Total PeCDF 13.0 -
<br />1,2,3,4,7,8,9-HpCDF 1.51 - J 0.0151 0.0883 Total HxCDF 18.9 -
<br />OCDF 36.7 -0.0110 0.170 Total HpCDF 39.6 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 89.0 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 92.6 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 94.0 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 89.8 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 82.3 23.0 - 140
<br />13C-OCDD 65.1 17.0 - 157
<br />13C-2,3,7,8-TCDF 93.5 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 85.8 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 87.6 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 87.1 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 83.3 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 80.0 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 79.6 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 79.7 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 80.5 26.0 - 138
<br />13C-OCDF 68.7 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 84.1 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/18/2018 4/18/2018
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