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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-006-SA Date Extracted: 04-16-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-6 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 5.00
<br />Matrix: Solid Amount: 5.02 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4473 % Solids: 96.16
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.232 - 0.0273
<br />1,2,3,7,8-PeCDD 1.06 - J 1.06 0.0570
<br />1,2,3,4,7,8-HxCDD 1.72 - J 0.172 0.0793
<br />1,2,3,6,7,8-HxCDD 4.93 - J 0.493 0.0940 Total TCDD ND 0.232
<br />1,2,3,7,8,9-HxCDD 3.17 - J 0.317 0.0823 Total PeCDD 2.91 -J
<br />1,2,3,4,6,7,8-HpCDD 115 -1.15 0.0842 Total HxCDD 31.8 -
<br />OCDD 1070 -0.321 0.172 Total HpCDD 206 -
<br />2,3,7,8-TCDF 1.35 -0.135 0.0269
<br />1,2,3,7,8-PeCDF ND 0.269 -0.0449
<br />2,3,4,7,8-PeCDF 1.38 - J 0.414 0.0468
<br />1,2,3,4,7,8-HxCDF 2.27 - J 0.227 0.0437
<br />1,2,3,6,7,8-HxCDF 1.47 - J 0.147 0.0417
<br />2,3,4,6,7,8-HxCDF 1.81 - J 0.181 0.0574
<br />1,2,3,7,8,9-HxCDF 0.677 - J 0.0677 0.0657 Total TCDF 7.40 -
<br />1,2,3,4,6,7,8-HpCDF 27.9 -0.279 0.0747 Total PeCDF 13.2 -
<br />1,2,3,4,7,8,9-HpCDF 1.81 - J 0.0181 0.0883 Total HxCDF 39.9 -
<br />OCDF 65.4 -0.0196 0.170 Total HpCDF 78.0 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 89.9 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 90.5 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 94.1 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 92.4 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 89.5 23.0 - 140
<br />13C-OCDD 78.6 17.0 - 157
<br />13C-2,3,7,8-TCDF 93.0 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 86.3 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 87.1 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 88.4 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 85.6 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 85.4 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 84.8 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 87.3 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 88.6 26.0 - 138
<br />13C-OCDF 77.2 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 85.7 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/18/2018 4/18/2018
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