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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-007-SA Date Extracted: 04-16-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-7 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 1.65
<br />Matrix: Solid Amount: 5.05 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4473 % Solids: 95.81
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.251 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.356 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.431 -0.0793
<br />1,2,3,6,7,8-HxCDD 2.12 - J 0.212 0.0940 Total TCDD ND 0.251
<br />1,2,3,7,8,9-HxCDD 1.44 - J 0.144 0.0823 Total PeCDD 0.923 -J
<br />1,2,3,4,6,7,8-HpCDD 47.6 -0.476 0.0842 Total HxCDD 14.3 -
<br />OCDD 398 -0.119 0.172 Total HpCDD 84.9 -
<br />2,3,7,8-TCDF 1.43 -0.143 0.0269
<br />1,2,3,7,8-PeCDF ND 0.372 -0.0449
<br />2,3,4,7,8-PeCDF 0.725 - J 0.218 0.0468
<br />1,2,3,4,7,8-HxCDF 0.829 - J 0.0829 0.0437
<br />1,2,3,6,7,8-HxCDF 0.626 - J 0.0626 0.0417
<br />2,3,4,6,7,8-HxCDF 0.703 - J 0.0703 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.344 -0.0657 Total TCDF 6.16 -
<br />1,2,3,4,6,7,8-HpCDF 10.3 -0.103 0.0747 Total PeCDF 5.88 -
<br />1,2,3,4,7,8,9-HpCDF 0.832 - J 0.00832 0.0883 Total HxCDF 12.9 -
<br />OCDF 33.0 -0.00990 0.170 Total HpCDF 30.7 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 64.6 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 67.5 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 70.3 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 69.0 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 66.8 23.0 - 140
<br />13C-OCDD 59.2 17.0 - 157
<br />13C-2,3,7,8-TCDF 68.0 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 66.0 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 63.2 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 67.2 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 64.2 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 63.4 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 64.0 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 64.6 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 65.7 26.0 - 138
<br />13C-OCDF 60.0 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 60.6 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/18/2018 4/18/2018
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