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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-008-SA Date Extracted: 04-16-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-8 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 2.93
<br />Matrix: Solid Amount: 5.02 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4473 % Solids: 94.62
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.255 - 0.0273
<br />1,2,3,7,8-PeCDD 0.953 - J 0.953 0.0570
<br />1,2,3,4,7,8-HxCDD 0.934 - J 0.0934 0.0793
<br />1,2,3,6,7,8-HxCDD 2.85 - J 0.285 0.0940 Total TCDD ND 0.255
<br />1,2,3,7,8,9-HxCDD 1.73 - J 0.173 0.0823 Total PeCDD 4.11 -J
<br />1,2,3,4,6,7,8-HpCDD 54.9 -0.549 0.0842 Total HxCDD 24.4 -
<br />OCDD 453 -0.136 0.172 Total HpCDD 105 -
<br />2,3,7,8-TCDF 1.73 -0.173 0.0269
<br />1,2,3,7,8-PeCDF ND 0.387 -0.0449
<br />2,3,4,7,8-PeCDF 0.736 - J 0.221 0.0468
<br />1,2,3,4,7,8-HxCDF 0.886 - J 0.0886 0.0437
<br />1,2,3,6,7,8-HxCDF 0.699 - J 0.0699 0.0417
<br />2,3,4,6,7,8-HxCDF 0.803 - J 0.0803 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.281 -0.0657 Total TCDF 9.10 -
<br />1,2,3,4,6,7,8-HpCDF 9.38 -0.0938 0.0747 Total PeCDF 9.08 -
<br />1,2,3,4,7,8,9-HpCDF 0.802 - J 0.00802 0.0883 Total HxCDF 13.2 -
<br />OCDF 22.1 -0.00663 0.170 Total HpCDF 24.6 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 79.8 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 81.7 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 85.3 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 79.9 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 76.9 23.0 - 140
<br />13C-OCDD 60.1 17.0 - 157
<br />13C-2,3,7,8-TCDF 78.5 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 78.2 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 76.9 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 80.2 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 77.7 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 71.9 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 72.3 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 76.8 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 75.2 26.0 - 138
<br />13C-OCDF 63.7 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 75.5 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/18/2018 4/18/2018
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