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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-009-SA Date Extracted: 04-16-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-9 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 0.139
<br />Matrix: Solid Amount: 5.03 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4473 % Solids: 93.92
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.223 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.339 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.420 -0.0793
<br />1,2,3,6,7,8-HxCDD ND 0.431 -0.0940 Total TCDD ND 0.223
<br />1,2,3,7,8,9-HxCDD ND 0.390 -0.0823 Total PeCDD ND 0.339
<br />1,2,3,4,6,7,8-HpCDD 5.47 -0.0547 0.0842 Total HxCDD 1.72 -J
<br />OCDD 44.1 -0.0132 0.172 Total HpCDD 10.7 -
<br />2,3,7,8-TCDF 0.560 - J 0.0560 0.0269
<br />1,2,3,7,8-PeCDF ND 0.326 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.319 -0.0468
<br />1,2,3,4,7,8-HxCDF ND 0.349 -0.0437
<br />1,2,3,6,7,8-HxCDF ND 0.357 - 0.0417
<br />2,3,4,6,7,8-HxCDF ND 0.400 - 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.430 -0.0657 Total TCDF 1.15 -
<br />1,2,3,4,6,7,8-HpCDF 1.48 - J 0.0148 0.0747 Total PeCDF 0.564 -J
<br />1,2,3,4,7,8,9-HpCDF ND 0.308 -0.0883 Total HxCDF 0.710 -J
<br />OCDF 2.56 - J 0.000768 0.170 Total HpCDF 3.02 -J
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 88.8 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 93.2 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 92.2 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 90.3 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 86.3 23.0 - 140
<br />13C-OCDD 76.3 17.0 - 157
<br />13C-2,3,7,8-TCDF 93.2 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 89.7 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 91.8 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 86.5 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 82.3 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 81.4 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 83.1 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 82.9 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 87.8 26.0 - 138
<br />13C-OCDF 75.6 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 84.6 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/18/2018 4/18/2018
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