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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-010-SA Date Extracted: 04-16-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-10 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 1.23
<br />Matrix: Solid Amount: 5.06 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4473 % Solids: 93.98
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.237 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.493 -0.0570
<br />1,2,3,4,7,8-HxCDD 0.700 - J 0.0700 0.0793
<br />1,2,3,6,7,8-HxCDD 1.71 - J 0.171 0.0940 Total TCDD ND 0.237
<br />1,2,3,7,8,9-HxCDD 1.34 - J 0.134 0.0823 Total PeCDD ND 0.493
<br />1,2,3,4,6,7,8-HpCDD 35.6 -0.356 0.0842 Total HxCDD 13.4 -
<br />OCDD 285 -0.0855 0.172 Total HpCDD 63.3 -
<br />2,3,7,8-TCDF 1.16 -0.116 0.0269
<br />1,2,3,7,8-PeCDF ND 0.336 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.363 -0.0468
<br />1,2,3,4,7,8-HxCDF 0.791 - J 0.0791 0.0437
<br />1,2,3,6,7,8-HxCDF 0.644 - J 0.0644 0.0417
<br />2,3,4,6,7,8-HxCDF 0.736 - J 0.0736 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.356 -0.0657 Total TCDF 5.59 -
<br />1,2,3,4,6,7,8-HpCDF 7.49 -0.0749 0.0747 Total PeCDF 4.71 -J,M
<br />1,2,3,4,7,8,9-HpCDF ND 0.239 -0.0883 Total HxCDF 10.9 -
<br />OCDF 17.5 -0.00525 0.170 Total HpCDF 19.8 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 91.9 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 95.9 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 96.3 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 94.2 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 92.1 23.0 - 140
<br />13C-OCDD 80.8 17.0 - 157
<br />13C-2,3,7,8-TCDF 93.2 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 91.8 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 91.8 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 89.7 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 86.8 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 86.1 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 87.1 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 89.0 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 91.6 26.0 - 138
<br />13C-OCDF 81.5 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 89.8 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/18/2018 4/18/2018
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