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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-011-SA Date Extracted: 04-17-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-11 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 2.94
<br />Matrix: Solid Amount: 5.01 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4475 % Solids: 92.86
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.192 - 0.0273
<br />1,2,3,7,8-PeCDD 0.565 - J 0.565 0.0570
<br />1,2,3,4,7,8-HxCDD 0.956 - J 0.0956 0.0793
<br />1,2,3,6,7,8-HxCDD 2.57 - J 0.257 0.0940 Total TCDD ND 0.192
<br />1,2,3,7,8,9-HxCDD 1.68 - J 0.168 0.0823 Total PeCDD 3.01 -J
<br />1,2,3,4,6,7,8-HpCDD 61.1 -0.611 0.0842 Total HxCDD 19.0 -
<br />OCDD 556 -0.167 0.172 Total HpCDD 114 -
<br />2,3,7,8-TCDF 1.58 -0.158 0.0269
<br />1,2,3,7,8-PeCDF 0.472 - J 0.0142 0.0449
<br />2,3,4,7,8-PeCDF 1.11 - J 0.333 0.0468
<br />1,2,3,4,7,8-HxCDF 1.44 - J 0.144 0.0437
<br />1,2,3,6,7,8-HxCDF 1.04 - J 0.104 0.0417
<br />2,3,4,6,7,8-HxCDF 1.03 - J 0.103 0.0574
<br />1,2,3,7,8,9-HxCDF 0.694 - J 0.0694 0.0657 Total TCDF 9.88 -
<br />1,2,3,4,6,7,8-HpCDF 13.5 -0.135 0.0747 Total PeCDF 11.5 -
<br />1,2,3,4,7,8,9-HpCDF 1.14 - J 0.0114 0.0883 Total HxCDF 18.6 -
<br />OCDF 29.9 -0.00897 0.170 Total HpCDF 35.7 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 96.8 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 100 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 105 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 99.9 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 93.6 23.0 - 140
<br />13C-OCDD 76.3 17.0 - 157
<br />13C-2,3,7,8-TCDF 99.9 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 98.5 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 99.3 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 95.2 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 93.2 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 91.4 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 91.1 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 91.7 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 92.2 26.0 - 138
<br />13C-OCDF 77.7 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 89.3 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/19/2018 4/19/2018
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