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110 2nd Avenue South,#D7 Pachew CA 94553-5560 <br /> Inc.McCampbell Analytical, Telephone 925-798-1620 Fax 925 798-1622 <br /> A# I Website www mccampliell corn E-mail main mccampbell com <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> 837 Shaw Road <br /> Date Received 01/23/04 <br /> Client Contact Tun Cuellar Date Extracted 01123104-01/26/04 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 01/23/04-01/26/04 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0401260 <br /> Lab ID 0401260-025A 0401260-026A ` <br /> Client ID P43-30' P4345' <br /> Reporting Limit for <br /> DF=1 <br /> Matrix S S <br /> DF 2 1 W <br /> Compound Concentration Vg/Kg ug/L <br /> tert-Amyl methyl ether(TAME) ND<10 ND 50 05 <br /> t-Butyl alcohol(TBA) ND<50 ND 25 50 <br /> 1,2-Dibromoethane(EDB) ND<10 ND 50 05 <br /> 1 2-Dichloroethane(1,2-DCA) ND<10 ND 50 05 <br /> Dusopropyl ether(DIPS) ND<10 ND 5 0 05 <br /> Ethyl tert-butyl ether(ETBE) ND<10 ND 5 0 0 5 <br /> Methyl-t-butyl ether(MTBE) 390 ND 5 0 05 <br /> Surrogate Recoveries(%) <br /> %SS 923 887 <br /> Comments <br /> 'water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples inµg/kg wipe samples in lxg/wtpe, <br /> product/oil/non-aqueous liquid samples in mp/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water Immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> o anic content <br /> DHS Certification No 1644 C"VvAngela Rydelius,Lab Manager <br />