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110 2nd Avenue South,#D7 Pacheco,CA 94553-5560 <br /> McCampbell_Analytical, Inc. Telephone 925-7981620 Fax 925-7981622 <br />-- - - ,� - - - - - - -_ -- Website wwwmecampbell corn-E trail main Jinceampbell corn- <br /> Advanced <br /> ornAdvanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01120/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> • Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 01/24/04-01128/04 <br /> Senu-Volatile Organics by GUMS(Basic Target List)* <br /> Extraction Method SW3510C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-008D <br /> Client ID P39-36to41 --- - <br /> Matrix Water <br /> Compound Concentration * DF R`Lmt Compound Concentration* DF Re <br /> La mg <br /> T.nsi <br /> Acenaphthene ND 10 10 Acenaphthylene ND 1 0 10 <br /> Anthracene ND 10 10 Benzidine ND 10 50 <br /> Benzoic Acid ND 10 50 Benzo(a)anthracene ND 1 0 10 <br /> Benzo b fluoranthene ND 1 0 10 Benzo k fluoranthene ND 1 0 10 <br /> Benzo( ,h,i) a lene ND 1 0 10 Benzo(a) a ND 1 0 10 <br /> Benzyl Alcohol ND 1 0 20 Bis 2�hloroethoxy)Methane ND 1 0 10 <br /> Bis 2-chloroeth 1 Ether ND 1 0 10 Bis(2-chloroiso ro 1)Ether ND 1 0 10 <br /> Bis 2-eth ]hex 1)Phthalate ND 1 0 10 4-Bromo hen 1 Phenyl Ether ND 1 0 10 T <br /> Butylbenzyl Phthalate ND 1 0 10 4-Chloroanllmc ND 1 o 20 <br /> 4-Chloro-3-meth 1 henoi ND 1 0 10 2-Chiorona hthalene ND 1 0 10 <br /> 2-Chlorophenol ND 10 10 4-Chloro hen 1 Phenyl Ether ND 1 0 10 <br /> Chrysene ND 10 10 Dibenzo(a,h)anthracene ND 10 10 <br /> Dibenzofuran ND 1 0 10 Di-n-butyl Phthalate ND 10 10 <br /> I2-Dichlorobenzene ND 10 10 1,3-Dichlorobenzene ND 10 10 <br /> 1,4-Dichlorobenzene ND 10 10 3,3-Dichlorobenzidine ND 1 0 20 <br /> 2,4-Dichlorohenol ND 10 10 Diethyl Phthalate ND to t0 <br /> 2 4-Dimeth 1 henol ND to 10 Dimethyl Phthalate ND 1 0 10 <br /> 4,6-Dimtro-2-methyl henoi ND 10 50 2,4-Dmitro henol ND 10 50 <br /> 2,4-Dmitrotoluene ND 10 10 2,6-Dinitrotoluenc ND 10 l0 <br /> Di-n-oc I Phthalate ND 1 0 10 1,2-Di hen lh drazine ND 1 0 10 <br /> Fluoranthene ND 10 10 Fluorene ND 10 10 <br /> Flexachlorobenzene ND 10 10 1-lexachiorobutadiene ND 10 10 <br /> 1lexachloroc clo entadiene ND 1 0 50 1lexachloroethane ND 1 0 10 <br /> Indeno 1,2,3-cd ene ND 10 10 Iso horone ND 10 l0 <br /> 2-Meth ina hthalene ND 10 10 2-Meth I hero]{o-Cresol) ND to 10 <br /> 3 Wor 4-Meth I henoi(m, -Cresol) ND 10 10 Naphthalene ND 1 0 10 <br /> 2-Nitroanilme ND 10 50 3-Nitroaniline ND 10 S0 <br /> 4-Nitroaniline ND 10 50 Nitrobenzene ND 10 50 <br /> 2-Nitrophenol ND 10 50 4-Nitrophenol ND 1 0 10 <br /> N-Nitrosodi hen lamme ND 10 10 N-Nitrosodi-n-propylamine ND 1 0 10 <br /> Pentachlorophenol ND 10 50 Phenanthrene ND l 0 10 <br /> Phenol ND 10 10 Pyrene ND 10 16 <br /> 1,2,4-Trichlorobenzene ND 10 10 2,4 5-Tnchioro henol ND to 10 <br /> 2,4 6-Trichlorophenol ND to 10 <br /> Surrogate Recoveries <br /> %SSI 941 %SS2 987 <br /> %SS3 924 %SS4 972 <br /> %SS5 867 %SS6 889 <br /> Comments i <br /> *water samples and all TCLP&SPLP extracts are reported 1n Vg/L,soil/sludge/solid samples in mg/kg,wipe samples in gglwipe,productloil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification Na 1644 L)1 Angela Rydellus,Lab Manager <br />