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110 2nd Avenue South,#137 Pacheco,CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br /> _Website www mceanipbell com h mail mamQmccampbell com., <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01120104-01122104 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 n <br /> Client P O Date Analyzed 01/24/04-01/28104 <br /> Semi-Volatile Organics by GCIMS(Basic l arget List)* <br /> Extraction Method SW3510C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-004D <br /> _- _ - - = Client ID - P42-40to44 - <br /> Matrix Water <br /> rt <br /> Compound Concentration * DF R`pum,m& Compound Concentration * DF R` n„t g <br /> Acenaphthene ND 1 0 10 _Acenaphthylene I ND 1 0 10 <br /> Anthracene ND 10 10 Benzidine I ND 10 50 <br /> Benzoic Acid ND 1 0 50 Benzo(a)anthracene ND 1 0 10 <br /> Benzo b)fluoranthene ND 1 0 10 Benzo k tluoranthene ND 1 0 10 <br /> Bcnza ,ham lene ND 1 0 10 Bcnza(a)pXrcne ND 10 10 <br /> Ben ]Alcohol ND 1 0 20 Bis(2-chloroethox )Methane ND 10 10 <br /> Bis(2-chloroeth l)Ether ND l 0 10 Sts(2-,Lh1oroiso ro l)Ether ND I 0 10 <br /> Bis 2-eth lhexyl)Phthalate ND 1 0 10 4-Bromo hen lY Phenyl Ether ND 1 0 10 <br /> But ]ben 1 Phthatate ND 1 0 10 4-Chloroanilme I ND 1 0 20 <br /> 4-Chloro-3-meth 7 henol ND 1 0 10 12-Chlorona hthalene ND ! 0 10 <br /> 2-Chlorophenol ND 10 10 4-Chloro hen l Pheny]Ether ND 10 10 <br /> Chrysene ND 10 I l0 Dibenza a h anthracene ND to I 10 <br /> Dibenzofuran ND 10 10 Di-n-butyl Phthalate ND 10 10 <br /> 1,2-Dichlorobenzene ND 10 10 1,3-Dichlorobenzene ND 10 10 <br /> 1,4-Dichlorobenzene ND 10 10 3,3-Dichlorobenzidine ND 10 20 <br /> 2,4-Dichloro henol ND 10 10 I Diethyl Phthalate ND 1 0 10 <br /> 2,4-Dimethylphenol ND 10 10 Dimethyl Phthalate ND 10 10 <br /> 4 6-Dmitro-2-meth I henol ND 10 50 2,4-Dimtrophenol ND to 50 <br /> 2,4-Dirntrotoluene ND 1 0 I 10 2,6-Dmitrotoluene ND 10 I to <br /> Di-n-octyl Phthalate ND 10 10 1 2-Di hen lh drazme ND 10 10 <br /> Fluoranthene ND l0 10 Fluorene ND 10 10 <br /> Hexachlorobenzene ND I 10 10 Hexachlorobutadiene ND 10 10 <br /> Hexachloroc clo entadiene ND 1 0 50 Hexachloroethane ND to 10 <br /> Indeno(I 2,3-cd)pyrene ND 10 10 Iso horone ND 1 0 10 <br /> 2-Meth lna hthalene ND 10 10 2-Meth l henol o-Cresol ND 1 0 10 <br /> 3&/or4-MethylphenoE m,p-Cresol) ND 10 10 Naphthalene ND t0 Ip <br /> 2-Nitroanilme ND 10 50 3-Nitroantlme ND l0 I 50 <br /> 4-Nitroaniline ND 10 50 Nitrobenzene ND 10 I 50 <br /> 2-Nitrophenol ND 1 10 50 14-Nitro henol ND 1 0 I 10 <br /> N-Nitrosodiphen lamme ND 10 10 N-Nitrosodi-n-propylamine ND I 10 10 <br /> Pentachlorophenol i ND 1 0 50 Phenanthrene ND I lo 10 <br /> Phenol ND 10 I 10 Pyrene ND l0 10 <br /> 1,2,4-Tnchlorobenzcne ND 10 10 . 2,4 5-Trichlorophenol ND I to to <br /> 2,4,6-Trichlorophenol ND to 10 <br /> Surrogate Recoveries(%) r <br /> %SS 1 999 %SS2 I 103 <br /> %SS3 91 8 %SS4 863 <br /> %SS5 88 1 %SS6 933 <br /> Comments i <br /> *water samples and all TCLP&SPLP extracts are reported m jig/L,soil/sludge/solid samples in mg/kg,wipe samples in Ag/wipe,product/oll/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than-2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />